2015
DOI: 10.3390/app5030415
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Expeditious Synthesis of Noble Metal Nanoparticles Using Vitamin B12 under Microwave Irradiation

Abstract: A greener synthesis protocol for noble nanometals is developed using vitamin B12 as a reducing and capping agent in conjunction with the use of microwaves. Successful assembly of nanoparticles or microparticles with varied shapes and sizes have been demonstrated. The synthesized Ag, Au, and Pd samples were thoroughly characterized with X-ray diffraction, scanning electron microscopy, transmission electron microscopy, high resolution transmission microscopy, and UV-visible spectrophotometry, confirming that met… Show more

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Cited by 15 publications
(3 citation statements)
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“…Generally, vitamins may work as capping as well as reducing agents in the green synthesis of nanomaterials. [41,42] Moreover, biodegradable polymers such as cellulose and hemicellulose functions as reducing and capping agents, and these factors may significantly influence the size, shape, and morphology of nanomaterials. Furthermore, the biological methods of nanomaterial synthesis are conducted via the incorporation of plant-based resources and microorganisms like bacteria, actinomycetes, algae, yeast and fungi.…”
Section: Properties Of Zinc Oxide Nanostructuresmentioning
confidence: 99%
“…Generally, vitamins may work as capping as well as reducing agents in the green synthesis of nanomaterials. [41,42] Moreover, biodegradable polymers such as cellulose and hemicellulose functions as reducing and capping agents, and these factors may significantly influence the size, shape, and morphology of nanomaterials. Furthermore, the biological methods of nanomaterial synthesis are conducted via the incorporation of plant-based resources and microorganisms like bacteria, actinomycetes, algae, yeast and fungi.…”
Section: Properties Of Zinc Oxide Nanostructuresmentioning
confidence: 99%
“…Another important vitamin exploited for the synthesis of NPs is vitamin B12. To synthesize Ag-NPs, Au-NPs, and Pd-NPs, vitamin B12 solution was mixed with silver nitrate, gold (III) chloride, and palladium acetate solutions, respectively [ 107 ]. All mixtures were tested in the presence and absence of microwave (MV) irradiation.…”
Section: Green Synthesis-based Systemsmentioning
confidence: 99%
“…This kind of limitation and interference can be avoided by using the potentiometric configuration that works at a negligible bias voltage as previously reported in the several studies [ 51 , 52 , 53 , 54 ]. The vitamin B 12 has been used as a reducing and capping agent for the preparation of noble metal nanoparticles [ 55 ].…”
Section: Introductionmentioning
confidence: 99%