Exfoliation of MoS2-RGO Hybrid 2D Sheets by Supercritical Fluid Process

Abstract

Layered 2D transition metal dichalcogenides (TMD’s) have been considered as an important class of materials in the field of energy and environmental applications. Therefore, it is desirable to fabricate 2D hybrid TMD’s materials in simple solution processing methods. In this study, MoS2-RGO hybrid 2D few layered sheets are produced by supercritical fluid process (SCF) by using ethanol as solvent at 250 ºC in a short duration of 0.5 h. Atomic force microscopy (AFM), transmission electron microscope (TEM) and scanning electron microscope (SEM) images confirmed the formation of 2D hybrid few layered sheets. The electrochemical impedance measurement indicates fivefold increase in conductivity of bulk MoS2. This work presents rapid and one pot exfoliation of MoS2 and simultaneous reduction of GO that can facilitate the production of 2D hybrid materials.

Photocatalytic Degradation of Rhodamine B Dye by Nanocomposites: A Review

“…A variety of possible photo-sensitive nano-semiconductor metal halide/oxides/sulphide, such as TiO2, ZnO, CuO, BiFeO3 and Carbon-based nanostructures have been produced and employed as photocatalysts for water purification, thanks to rapid advances in nanotechnology [11]. This innovative interdisciplinary branch of science and technology leads to the formation of different morphologies like nanoparticles [12-16][17], nanotubes [18,19], nanorods [20,21], nanocubes [22] and nanosheets [23] by using numerous advanced methods such as hydrothermal, solvothermal, sol-gel, microwave, co-precipitation methods [24] with different applications in many fields such as from basic chemistry [25][26][27][28], physics [29][30][31] to the advanced electronics [32][33][34][35][36], nanotechnology [37][38][39][40][41], biotechnology [42][43][44][45][46][47] by altering the properties like mechanical [17,48] physical [49][50][51] and magnetic [52,53] so they come up with an ideal of environmental friendly [54], with a motto of decreasing the pollutions [55,…”