The short-lived ruthenium nuclides produced in the spontaneous fission of 252 Cf were separated from the fission products mixture by SISAK coupled with a KCl/He gas-jet recoil-transport system and y-rays were measured on-line after a single extraction step. The energies and intensities of the y-rays following the β' decays of 107 ~ 112 Ru were determined. 0.2M H2S04 0.2M H2S04 5X10~5M RuCl, 0.015M Ce(S04)2 Fig. 1. Flow sheet of the SISAK chemical separation system for the fast separation of ruthenium. Dg, CI and FC stand for degasser, centrifuge and flow cell, respectively. The aqueous solutions are preheated to about 90°C.