“…Many analytical methods have been used in the determination of NF, including spectrophotometry, 6 fluorometry, 7 HPLC, 8 LC/MS, 9 capillary electrophoresis 10,11 and electrochemical analysis. 12,13 Among these methods, the electrochemical method with the advantage of simplicity, a fast response, high sensitivity and low cost has attracted more and more attentions. [14][15][16] Therefore, the electrochemical method is promising for NF analysis in complex matrices, especially for the biological samples.…”