Abstract:A series of W-type Ba-based Co-W ferrites with composition BaCoxCd2-xFe16O27 (x ═ 0.0, 0.1, 0.2, 0.3, 0.4 & 0.5) were fabricated by co-precipitation process at sintering 1100 °C for 8 h. In order to investigate structural, optical, electrical and magnetic properties XRD, FTIR, IV and VSM tools were employed to confirm the formation of ferrites phase. Crystallite size was observed in the range of 71.79 – 27.88 nm with the increase of cobalt contents to confirm the formation of W-type phase. FTIR investigate… Show more
“…All the samples were dissolved in deionized water to do the UV-Vis spectroscopy. The absorption coefficient of fabricated material was found using the following relation (10) [25].…”
The Nickel substituted Cu-Co-Zn-Ce nano ferrites, Zn0.15Co0.45Cu0.40-xNix Fe1.85Ce0.15O4 with x=0, 0.1, 0.20, 0.30, 0.40, were synthesized using the coprecipitation technique. The sample were sintered at 900 ℃ for 5h. The structural, electrical, dielectric and magnetic properties of all the prepared samples were characterized by XRD, SMU2401, UV-Vis and FTIR. The powder X-ray diffraction patterns of all the prepared samples confirmed the formation of single-phase cubic spinel structures. These samples further characterized for the electrical properties by using two-probe type method. The DC resistivity of all the ferrite composition decreased as the temperature increased, showing their semiconductor nature. UV-Vis and FTIR confirmed the substitution of nickel in Cu-Co-Zn-Ce ferrites. From UV-Vis it is observed that the optical band gap changes from 3.9 eV to 5.3 eV with addition of Ni. FTIR analysis revealed that a strong variation on tetrahedral absorption frequency band is present which is due to the replacement of Ni on Cu. All these results suggested that these materials can be used for wastewater treatment.
“…All the samples were dissolved in deionized water to do the UV-Vis spectroscopy. The absorption coefficient of fabricated material was found using the following relation (10) [25].…”
The Nickel substituted Cu-Co-Zn-Ce nano ferrites, Zn0.15Co0.45Cu0.40-xNix Fe1.85Ce0.15O4 with x=0, 0.1, 0.20, 0.30, 0.40, were synthesized using the coprecipitation technique. The sample were sintered at 900 ℃ for 5h. The structural, electrical, dielectric and magnetic properties of all the prepared samples were characterized by XRD, SMU2401, UV-Vis and FTIR. The powder X-ray diffraction patterns of all the prepared samples confirmed the formation of single-phase cubic spinel structures. These samples further characterized for the electrical properties by using two-probe type method. The DC resistivity of all the ferrite composition decreased as the temperature increased, showing their semiconductor nature. UV-Vis and FTIR confirmed the substitution of nickel in Cu-Co-Zn-Ce ferrites. From UV-Vis it is observed that the optical band gap changes from 3.9 eV to 5.3 eV with addition of Ni. FTIR analysis revealed that a strong variation on tetrahedral absorption frequency band is present which is due to the replacement of Ni on Cu. All these results suggested that these materials can be used for wastewater treatment.
“…It was observed that the dislocation density was increased with the addition of Zn from 4.06 × 10 -4 nm -2 to 6.46 × 10 -4 nm -2 , as presented in Table 1. The Braggs equation was used to determine the interplanar distance (d), that is given below [10][11][12][13];…”
Zin substituted Mg-Mn-Bi nano ferrites, Mg0.5 𝑀𝑀𝑀𝑀0.5−x 𝑍𝑍𝑍𝑍x 𝐵𝐵𝑖𝑖0.05Fe1.95O4 (x= 0, 0.125, 0.25, 0.375, 0.5) were synthesized using the sol gel auto combustion method. Structural parameters were analyzed through x-ray diffraction. It was revealed that all the samples are single phase spinel structure with Fd-3m space group and crystallite size, lattice constant and x-ray densities were varying with Zn concentration. RAMAN analysis showed the cation vibration. The DC resistivity was enhanced of all the samples with increasing concentration of Zn. The substitution of Zn also responsible for the variation of magnetic parameters as observed with VSM. Due to these remarkable properties all the prepared samples may be utilized at high frequency in microwave devices.
“…In order to make a kind of YM based bioink that can be solidified via a photo-crosslinking strategy, appropriate chemical modification was applied to this polysaccharide that make YM crosslinkable by light irradiation [35,36]. Methacryloyl groups were introduced onto the reactive hydroxyl groups of YM to obtain methacryloyl modified YM (YM-MA) by using the method described at 2.2.1.…”
Section: Synthesis and Characterization Of Three Novel Bioinks Derive...mentioning
3D bioprinting technology displays many advantages for tissue engineering applications, but its utilization is limited by veryfew bioinks available for biofabrication. In this study, a novel type of bioink, which includes three methacryloyl modifiedmannans, was introduced to 3D bioprinting for tissue engineering applications. Yeast mannan (YM) was modified by reactingwith methacrylate anhydride (MA) at different concentrations, and three YM derived bioinks were obtained, which weretermed as YM-MA-1, YM-MA-2 and YM-MA-3 and were distinguished with different adjusted methacrylation degrees. TheYM derived bioink displayed an advantage that the mechanical properties of its photo-cured hydrogels can be enhanced withits methacrylation degree. Hence, YM derived bioinks are fitted for the mechanical requirements of most soft tissueengineering, including cartilage tissue engineering. By selecting chondrocytes as the testing cells, well cytocompatibility of YM-MA-1, YM-MA-2 had been confirmed by CCK-8 method. Following photo-crosslinking and implantation into SD rats for 4 weeks, the in vivo biocompatibility of the YM-MA-2 hydrogel is acceptable for tissue engineering applications. Hence, YM-MA-2 was chosen for 3D bioprinting. Our data demonstrated that hydrogel products with designed shape and living chondrocytes have been printed by applying YM-MA-2 as the bioink carrying chondrocytes. After the YM-MA-2 hydrogel with encapsulated chondrocytes was implanted subcutaneously in nude mice for 2 weeks, GAG and COLII secretion was confirmed by histological staining in YM-MA-2-H, indicating that the YM derived bioink can be potentially applied to tissue engineering by employing a 3D printer of stereolithography.
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