Effects of Grain Boundary Geometry and Boron Addition on the Local Mechanical Behavior of Interstitial-Free (IF) Steels

Abstract

Nanoindentation measurements on various grain boundaries were performed to clarify the effects of the geometry of neighboring grains and the addition of boron (B) on plasticity resistance in the vicinity of grain boundaries in interstitial free (IF) steels. We define a parameter, ¡, which is measured by the slope of a P/hh curve with load, P, and displacement, h, to estimate the resistance against plastic deformation in the grain interior and at the grain boundaries. The value of ¡ is almost constant with the geometric compatibility factor of the grain boundaries. This result shows that the geometry of the neighboring grains does not affect the plasticity resistance of the grain boundaries. However, the value of ¡ increases by the addition of B due to the segregation of B and Ti to the grain boundaries. It is indicated that the elemental segregation to the grain boundaries enhances the resistance to the plastic deformation in the vicinity of the grain boundaries.

Hardness–Deformation Energy Relationship in Metals and Alloys: A Comparative Evaluation Based on Nanoindentation Testing and Thermodynamic Consideration

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Quantitative Characterization by Transmission Electron Microscopy and Its Application to Interfacial Phenomena in Crystalline Materials

“…The pile-up model is widely accepted for understanding the Hall-Petch relationship [118], and the grain boundarydislocation interaction has been investigated from both experimental and computational viewpoints . Recently, nanoindentation techniques have been employed to understand the mechanical response in the vicinity of an individual grain boundary [128][129][130][131][132][133][134][135][136][137][138][139][140][141][142][143]. Moreover, in situ TEM (and SEM) straining experiments are powerful tools for understanding the microstructure evolution of small-scale specimens under the stress field.…”