Effect of the Operational Conditions in the Characteristics of Ceramic Foams Obtained from Quartz and Sodium Silicate

Abstract

Ceramic foams were fabricated without using melting pots through the direct foaming of compacted powder mixtures of commercial quartz (SiO2) with fluxing agents (Na2CO3 and CaO) and a foaming agent (Na2SiO3·5H2O) at a relatively low temperature range (850−870 °C). The effects of the pressing pressure of the powders, the foaming time, foaming temperature, and mixture content were evaluated. The obtained cellular solid materials presented an acceptable volumetric expansion at a pressing pressure of 4 t. The materials only presented porosity at a minimum temperature of 850 °C and at a minimum time of 30 min. All the foamed samples showed an acceptable symmetric expansion and non-appreciable fissures. The study of the mixture content through the statistical software MODDE® shows that the porosity of the samples was principally affected by the Na2SiO3 content and the foaming temperature. The samples obtained at the optimum controlling factors proposed by this statistical software presented an apparent density, porosity, and mechanical strength of 1.09 ± 0.03 g/cm3, 56.01% ± 1.12%, and 3.90 ± 0.16 MPa, respectively. Glass and ceramics foams such as those obtained in this work become attractive as insulation materials in applications where high temperatures occur due to their higher melting points.

Comparison of Toughening Effects of Various Additives on Phenolic Foam

“…The toughening ability of sodium silicate (SS) has also been analyzed in this work. SS is usually used as an alternative blowing agent − or a precursor for silica production . Phenol–urea–formaldehyde resin has been extensively studied for various applications such as adhesive and foam making. , Urea (U) was added to the resin to reduce the residual formaldehyde content.…”