“…In order to prevent the formation of calcium carbonate as a second phase, nitrogen gas was constantly bubbled to the system. In the sequence, this mixture was transferred to a Teflon autoclave, which was finally sealed and placed in the MH system using 2.45 GHz microwave radiation with maximum power of 800 W [20] The MH conditions were kept at 140 C for 30 min, using a heating rate fixed at 10 C min À1 . Finalized the MH processing, the autoclave was naturally cooled at room temperature.…”