2001
DOI: 10.1111/j.1151-2916.2001.tb00903.x
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Dispersion and Slip Casting of Hydroxyapatite

Abstract: The dispersibility in deionized water of hydroxyapatite (HA) synthesized by a high-temperature (1000°C) solid-state reaction between tricalcium phosphate and calcium hydroxide was investigated as a function of the pH of the medium and the quantity of two dispersing agents (A ‫؍‬ inorganic, B ‫؍‬ organic) added to the slips. Although pH modification had a negligible effect on dispersibility, both of the dispersing agents produced a good dispersion at considerably higher concentrations (>2 wt% of HA). At optimum… Show more

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Cited by 51 publications
(26 citation statements)
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“…The relative densities of the samples are summarized in Table 1. It should be observed that the HA density value is within the range of similar packed hydroxyapatite green bodies obtained by a similar method and with starting powders of the same particle size [25]. In the case of HA10Y, due to the difference in the particle sizes, a better packing is achieved and consequently a higher green density is measured.…”
Section: Materials Processingmentioning
confidence: 53%
“…The relative densities of the samples are summarized in Table 1. It should be observed that the HA density value is within the range of similar packed hydroxyapatite green bodies obtained by a similar method and with starting powders of the same particle size [25]. In the case of HA10Y, due to the difference in the particle sizes, a better packing is achieved and consequently a higher green density is measured.…”
Section: Materials Processingmentioning
confidence: 53%
“…Since calcium orthophosphates are either thermally unstable (MCPM, MCPA, DCPA, DCPD, OCP, ACP, CDHA) or have a melting point at temperatures exceeding ~ 1400 °C with a partial decomposition (α-TCP, β-TCP, HA, FA, TTCP), only the first and the second consolidation approaches are used to prepare bulk bioceramics and scaffolds. The methods include uniaxial compaction [198,199], isostatic pressing (cold or hot) [200][201][202][203][204][205][206], granulation [207,208], loose packing [209], slip casting [210][211][212][213], gel casting [188,189,[214][215][216][217][218][219], pressure mold forming [220], injection molding [221], polymer replication [222][223][224][225], extrusion [226][227][228], slurry dipping and spraying [229], as well as to form ceramic sheets from slurries tape casting [124,216,230,231] doctor blade [232] and colander methods might be employed [194][195][196][197]…”
Section: Forming and Shapingmentioning
confidence: 99%
“…1,2 Many efforts have been made in order to improve the mechanical properties of HA and several forming techniques have been used. In addition to common pressing method (uniaxial, 3 hot pressing, 4 hot isostatic pressing 5 ), other methods have been proposed, such as slip-casting, 6,7 tape-casting, 8,9 injection moulding 10 and viscous plastic processing. 11 Colloidal processing offers the potential to produce reliably ceramic films and bulk forms through careful control of the initial suspension "structure" and its evolution during fabrication.…”
Section: Introductionmentioning
confidence: 99%