O(BO 3 ) 3 (GdCOB), single crystal caused by γ -irradiation were investigated.The crystal was exposed to γ -radiation of a dose up to 2 MGy. The changes in frequencies of piezoelectric resonances were registered with variation of the dose for two crystal plates: (XY) and (ZX) vibrating in longitudinal modes. The relationship between the radiation dose and the elastic coefficients s E 11 , s E 22 as well as the piezoelectric coefficients d 31 , d 12 was found. GdCOB crystal can be recommended for application in high-dose dosimetry.