Determination of volatile components of saffron by optimised ultrasound-assisted extraction in tandem with dispersive liquid–liquid microextraction followed by gas chromatography–mass spectrometry

Sereshti, Hassan; Heidari, Reza; Samadi, Soheila

doi:10.1016/j.foodchem.2013.08.024

Cited by 89 publications

(34 citation statements)

References 33 publications

Supporting

Mentioning

Contrasting

Unclassified

Order By: Relevance

“…Chloroform was found to be the best solvent for the extraction of safranal. Ultrasound assisted extraction in conjunction with dispersive liquid–liquid microextraction (DLLME) was chosen for the extraction of safranal by Sereshti and co‐workers . The extraction parameters, such as composition of extraction solvent, volume of preconcentration solvent and duration of sonication were optimized by using a half‐fraction factorial central composite design (CCD).…”

Section: Analysis Of Saffron Apocarotenoidsmentioning

confidence: 99%

See 1 more Smart Citation

Latest advances in the extraction and determination of saffron apocarotenoids

Kyriakoudi

2018

Electrophoresis

View full text Add to dashboard Cite

Saffron, the dried red stigmas of Crocus sativus L. plant, is the most expensive spice in the world. It is highly valued not only for the color and flavor that exerts to various foods and drinks but also for its functional properties. Various classes of apocarotenoids such as crocetin sugar esters, picrocrocin and safranal are responsible for these characteristics. In the present review, the evolution of the methods proposed by the ISO standard for extraction and determination of saffron apocarotenoids since 1980 is presented in parallel to other approaches proposed by various scientists to overcome limitations of the standard. Moreover, the latest advances regarding applications of novel extraction techniques and powerful analytical tools that require limited or no sample preparation are critically discussed.

show abstract

Section: Analysis Of Saffron Apocarotenoidsmentioning

confidence: 99%

“…Apart from HPLC, GC hyphenated with MS or not, has been also used over the years for the determination of safranal considering its volatile nature .…”

Section: Analysis Of Saffron Apocarotenoidsmentioning

confidence: 99%

Latest advances in the extraction and determination of saffron apocarotenoids

Kyriakoudi

2018

Electrophoresis

View full text Add to dashboard Cite

show abstract

“…The organic solvent is not retained by the highly polar silica surface and so is readily eluted from the cartridge. [47][48][49] …”

Section: Liquid-liquid Extractionmentioning

confidence: 99%

On-Line Sample Pre-Treatment Procedures Applied to LC–MS

Edge¹,

Herman²

2015

Fast Liquid Chromatography–Mass Spectrometry Methods in Food and Environmental Analysis

View full text Add to dashboard Cite

“…Because traditional one-factor-at-a-time optimization methods cannot examine the interaction of variables, experimental designs, such as central composite design (CCD) and the Box-Behnken design (BBD), have been widely adopted to evaluate the primary effect as well as the interactions and significance of each variable [31,45,46]. Because traditional one-factor-at-a-time optimization methods cannot examine the interaction of variables, experimental designs, such as central composite design (CCD) and the Box-Behnken design (BBD), have been widely adopted to evaluate the primary effect as well as the interactions and significance of each variable [31,45,46].…”

Section: Introductionmentioning

confidence: 99%