Determination of sulfonamide antibiotics and metabolites in liver, muscle and kidney samples by pressurized liquid extraction or ultrasound-assisted extraction followed by liquid chromatography–quadrupole linear ion trap-tandem mass spectrometry (HPLC–QqLIT-MS/MS)

Hoff, Rodrigo Barcellos; Pizzolato, Tânia Mara; Peralba, Maria do Carmo Ruaro; Díaz-Cruz, M. Silvia; Barceló, Damià

doi:10.1016/j.talanta.2014.10.045

Cited by 66 publications

(30 citation statements)

References 47 publications

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“…In the case of animal tissue samples, SLE [31][32][33], ASE [34][35][36], QuEChERS extraction [37,38], SALLE [40,41], and SPE [42] were the most reported methodologies for the extraction of SAs, along with other antibiotic or veterinary drugs, followed by reports of USE [36], DSPE [45], and SBSE [48]. Reports of on-line techniques include a fully automated on-line QuEChERS extraction protocol [39] and an on-line SPME protocol that utilized molecularly imprinted monolithic capillary columns [47].…”

Section: Discussionmentioning

confidence: 99%

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Food Sample Preparation for the Determination of Sulfonamides by High-Performance Liquid Chromatography: State-of-the-Art

et al. 2018

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Antibiotics are a common practice in veterinary medicine, mainly for therapeutic purposes. Sectors of application include livestock farming, aquacultures, and bee-keeping, where bacterial infections are frequent and can be economically damaging. However, antibiotics are usually administered in sub-therapeutic doses as prophylactic and growth promoting agents. Due to their excessive use, antibiotic residues can be present in foods of animal origin, which include meat, fish, milk, eggs, and honey, posing health risks to consumers. For this reason, authorities have set maximum residue limits (MRLs) of certain antibiotics in food matrices, while analytical methods for their determination have been developed. This work focuses on antibiotic extraction and determination, part of which was presented at the "1st Conference in Chemistry for Graduate, Postgraduate Students and PhD Candidates at the Aristotle University of Thessaloniki". Taking a step further, this paper is a review of the most recent sample preparation protocols applied for the extraction of sulfonamide antibiotics from food samples and their determination with high-performance liquid chromatography (HPLC), covering a five-year period.

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Section: Discussionmentioning

confidence: 99%

“…The lower phase was used for analysis. Although both developed protocols could efficiently extract the SAs from the tissue samples, UAE is simpler and less solvent and time-consuming [36].…”

Section: Slementioning

confidence: 99%

Food Sample Preparation for the Determination of Sulfonamides by High-Performance Liquid Chromatography: State-of-the-Art

et al. 2018

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“…Seu uso ainda é muito frequente na medicina veterinária, na área de produção animal e principalmente como profilático de infecções na produção em larga escala de aves e suínos (HOFF et al, 2015).…”

Section: Introductionunclassified

Monitoramento De Resíduos De Medicamentos Veterinários Em Alimentos E No Ambiente: Modelo Para Avaliação

Hoff¹

2018

SCI. ANIM. HEALTH

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O trabalho apresenta uma proposta para elencar prioridades na pesquisa de resíduos de fármacos de uso veterinário utilizados em larga escala na produção animal, tanto em alimentos destinados ao consumo humano como no ambiente. Para exemplificar o modelo proposto, adotou-se neste trabalho o caso específico das sulfonamidas, analisando-se as apresentações farmacêuticas disponíveis no mercado veterinário nacional em dois momentos distintos (2007 e 2017). Segundo o modelo proposto, pode-se dizer que o mesmo é adequado para subsidiar políticas regulatórias e delineamentos de experimentos de métodos de monitoramento de resíduos de medicamentos.

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“…Few studies have analyzed SAs and their metabolites in biological samples such as animal tissues (Hoff, Pizzolato, Peralba, Díaz-Cruz, & Barceló, 2015;Hou, Wu, Yang, & Du, 2013;Zhao et al, 2014), aquatic products (Kung, Tsai, Ku, & Wang, 2015), baby food (Aguilera-Luiz et al, 2012), honey (Juan-Borrás, Periche, Domenech, & Escriche, 2015), and milk (Han et al, 2013). Therefore, more efforts are needed in this regard.…”

Section: Introductionmentioning

confidence: 99%

Monitoring of twenty-two sulfonamides in edible tissues: Investigation of new metabolites and their potential toxicity

Abdallah¹,

Arnaudguilhem²,

Haifa

et al. 2016

Food Chemistry

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Determination of sulfonamide antibiotics and metabolites in liver, muscle and kidney samples by pressurized liquid extraction or ultrasound-assisted extraction followed by liquid chromatography–quadrupole linear ion trap-tandem mass spectrometry (HPLC–QqLIT-MS/MS)

Cited by 66 publications

References 47 publications

Food Sample Preparation for the Determination of Sulfonamides by High-Performance Liquid Chromatography: State-of-the-Art

Food Sample Preparation for the Determination of Sulfonamides by High-Performance Liquid Chromatography: State-of-the-Art

Monitoramento De Resíduos De Medicamentos Veterinários Em Alimentos E No Ambiente: Modelo Para Avaliação

Monitoring of twenty-two sulfonamides in edible tissues: Investigation of new metabolites and their potential toxicity

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