This 260 Series is dedicated to the dissemination of information on all phases of the preparation of the NBS uranium isotopic SRM for nondestructive assay. In general, much more detail will be found in this 260 than is generally allowed, or desirable, in scientific journal articles. This enables the user to assess the validity of processes employed, and to learn details of methods utilized for work entailing the greatest care. It is hoped that this 260 will provide sufficient additional information not found on the certificate so that new applications of these SRM's may be found.