“…The advent of a new era of materials science is manifested by unearthing of nanomaterials with applications in electronics, sensors, electrocatalysis, optoelectronics, biorelated applications field, and so forth. − These nanosized materials allow us to tailor their physical properties by varying experimental conditions, thus enabling their application in various fields. Further, it is conducive to employ rather green synthesis protocols for these nanostructures utilizing environmentally friendly precursors and medium. , Among the nanomaterials, 2D layered materials (graphene and its analogues, like transition metal dichalcogenides) have grabbed greater attention due to their distinctive material properties and their applicability in sensors, electronics, catalysis, energy-storage, and optoelectronic fields. − Among transition dichalcogenides, molybdenum disulfide (MoS 2 ) displays highest conductivity and has not shown scalability and economic issues to a large extent. − Various reported synthetic procedures for MoS 2 are micromechanical exfoliation, liquid phase exfoliation, physical vapor deposition, chemical solution process, chemical vapor deposition, etc.…”