Current trends in sample preparation by solid-phase extraction techniques for the determination of antibiotic residues in foodstuffs: a review

Khatibi, Seyed Amin; Hamidi, Samin; Siahi-Shadbad, Mohammad Reza

doi:10.1080/10408398.2020.1798349

Cited by 63 publications

(19 citation statements)

References 130 publications

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“…Confirmatory methods are essentially chromatographic methods (mainly liquid chromatography) coupled to mass spectrometry or ultraviolet (UV) [1]. However, capillary electrophoresis (CE) [65], CElaser-induced fluorescence [66], surface-enhanced Raman spectroscopy [67], and high-performance liquid chromatography (HPLC) with spectroscopic fluorometric detection (HPLC-RF) or with a spectroscopic HPLC-photodiode array detector [42] are also shown to be effective detectors of antibiotic residues.…”

Section: Confirmatory Methodsmentioning

confidence: 99%

The public health issue of antibiotic residues in food and feed: Causes, consequences, and potential solutions

et al. 2022

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Antibiotics are among the essential veterinary medicine compounds associated with animal feed and food animal production. The use of antibiotics for the treatment of bacterial infections is almost unavoidable, with less need to demonstrate their importance. Although banned as a growth factor for a few years, their use in animals can add residues in foodstuffs, presenting several environmental, technological, animal health, and consumer health risks. With regard to human health risks, antibiotic residues induce and accelerate antibiotic resistance development, promote the transfer of antibiotic-resistant bacteria to humans, cause allergies (penicillin), and induce other severe pathologies, such as cancers (sulfamethazine, oxytetracycline, and furazolidone), anaphylactic shock, nephropathy (gentamicin), bone marrow toxicity, mutagenic effects, and reproductive disorders (chloramphenicol). Antibiotic resistance, which has excessively increased over the years, is one of the adverse consequences of this phenomenon, constituting a severe public health issue, thus requiring the regulation of antibiotics in all areas, including animal breeding. This review discusses the common use of antibiotics in agriculture and antibiotic residues in food/feed. In-depth, we discussed the detection techniques of antibiotic residues, potential consequences on the environment and animal health, the technological transformation processes and impacts on consumer health, and recommendations to mitigate this situation.

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Section: Confirmatory Methodsmentioning

confidence: 99%

The public health issue of antibiotic residues in food and feed: Causes, consequences, and potential solutions

et al. 2022

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“… Schematic procedure of the dispersive liquid-liquid microextraction technique (the image is from [ 39 ]). …”

Section: Figurementioning

confidence: 99%

Recent Advances and Perspectives on the Sources and Detection of Antibiotics in Aquatic Environments

Zeng

Chang

Liu

et al. 2022

Journal of Analytical Methods in Chemistry

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Water quality and safety are vital to the ecological environment, social development, and ecological susceptibility. The extensive use and continuous discharge of antibiotics have caused serious water pollution; antibiotics are widely found in freshwater, drinking water, and reservoirs; and this pollution has become a common phenomenon and challenge in global water ecosystems, as water polluted by antibiotics poses serious risks to human health and the ecological environment. Therefore, the antibiotic content in water should be identified, monitored, and eliminated. Nevertheless, there is no single method that can detect all different types of antibiotics, so various techniques are often combined to produce reliable results. This review summarizes the sources of antibiotic pollution in water, covering three main aspects: (1) wastewater discharges from domestic sewage, (2) medical wastewater, and (3) animal physiology and aquaculture. The existing analytical techniques, including extraction techniques, conventional detection methods, and biosensors, are reviewed. The electrochemical biosensors have become a research hotspot in recent years because of their rapid detection, high efficiency, and portability, and the use of nanoparticles contributes to these outstanding qualities. Additionally, the comprehensive quality evaluation of various detection methods, including the linear detection range, detection limit (LOD), and recovery rate, is discussed, and the future of this research field is also prospected.

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“…In sample preparation, most of the commonly used methods for the analysis of veterinary drug residue in foods were liquid-liquid extraction, solid phase extraction, but the operations were complicated and timeconsuming. Quick, Easy, Cheap, Effective, Rugged, and Safe is a rapid pre-treatment method developed in recent years, which can be used to extract the target compound from the samples by a convenient, economical and rapid way (16)(17)(18). The main applications of quantitative multi-analyte methods in determination of veterinary drug residues in milk and other animal derived foods are presented in Table 1.…”

Section: Introductionmentioning

confidence: 99%

Rapid determination of 103 common veterinary drug residues in milk and dairy products by ultra performance liquid chromatography tandem mass spectrometry

Guo

Tian²,

Yang

et al. 2022

Front. Nutr.

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A multi-residue method has been developed for the identification and quantification of 103 common veterinary drug residues in milk and dairy Products. This method was based on QuEChERS with dispersive solid-phase where C18 sorbent and anhydrous sodium sulfate were used to sample purification. After evaporation and reconstitution, the samples were analyzed by ultra-performance liquid chromatography-tandem mass spectrometry. The mean recovery results were all higher than 60% except ampicillin, pipemidic acid, enoxacin, and estriol, and the relative standard deviation was <20.0%. The limit of quantification ranged between 0.1 and 5 μg/kg for milk and between 0.5 and 25 μg/kg for milk powder. It was successfully used to detect residues of veterinary drug in real samples. This study proposes a simple and fast analytical method for monitoring multi-class veterinary drug residues to ensure food safety.

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Current trends in sample preparation by solid-phase extraction techniques for the determination of antibiotic residues in foodstuffs: a review

Cited by 63 publications

References 130 publications

The public health issue of antibiotic residues in food and feed: Causes, consequences, and potential solutions

The public health issue of antibiotic residues in food and feed: Causes, consequences, and potential solutions

Recent Advances and Perspectives on the Sources and Detection of Antibiotics in Aquatic Environments

Rapid determination of 103 common veterinary drug residues in milk and dairy products by ultra performance liquid chromatography tandem mass spectrometry

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