Crystal structure of 1-(4-fluorophenyl)-N-(5-((triphenylstannyl)thio)thiophen-2-yl)methanimine, C₂₇H₂₀FN₃S₂Sn

Abstract

C 27 H 20 FN 3 S 2 Sn, monoclinic, P2 1 /n (no. 14), a = 15.631 (4) CCDC no.: 1580160The crystal structure is shown in the figure. Tables 1 and 2 contain details on crystal structure and measurement conditions and a list of the atoms including atomic coordinates and displacement parameters. Source of materialsThe ligand: 5-((4-fluorobenzylidene)amino)thiophene-2-thiol was synthesized by 4-fluorobenzaldehyde and 5-aminothiophene-2-thiol by refluxing in ethanol for 2 h (yellow solid). The organic ligand and triphenyltin chloride were added to benzene and sodium ethoxide, refluxed for