Cooling assisted headspace microextraction by packed sorbent coupled to HPLC for the determination of volatile polycyclic aromatic hydrocarbons in soil

Serenjeh, Fariba Nazari; Hashemi, Payman; Ghiasvand, Alireza; Rasolzadeh, Fahimeh; Heydari, Nahid; Badiei, Alireza

doi:10.1016/j.aca.2020.05.067

Cited by 22 publications

(7 citation statements)

References 22 publications

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“…(A) Schematic illustration of cooling assisted headspace MEPS method, and (B) evaluation the effect of reducing solid phase temperature on extraction efficiency. Reproduced from [189] with permission from Elsevier…”

Section: Applications Of Porous Framework In Microextraction Techniquesmentioning

confidence: 99%

“…In 2020, Nazari Serenjeh and co‐workers [189] proposed an MEPS method in the headspace of soil samples for extraction of volatile PAHs. The schematic of the proposed method is shown Figure 6A.…”

Section: Applications Of Porous Framework In Microextraction Techniquesmentioning

confidence: 99%

“…F I G U R E 6 (A) Schematic illustration of cooling assisted headspace MEPS method, and (B) evaluation the effect of reducing solid phase temperature on extraction efficiency. Reproduced from [189] with permission from Elsevier sample preparation techniques. Wang et al [198] employed two microporous zeolites (ZSM-5 and SAPO-34) for fabrication of hybrid adsorbent with PDMS polymer.…”

mentioning

confidence: 99%

“…The extraction performance of ZSM-5/PDMS (20:80 wt%) hybrid adsorbent due to synergic effect was higher than the pure zeolites or PDMS film. In 2020, Nazari Serenjeh and co-workers [189] proposed an MEPS method in the headspace of soil samples for extraction of volatile PAHs. The schematic of the proposed method is shown Figure 6A.…”

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confidence: 99%

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Applications of porous frameworks in solid‐phase microextraction

Khataei

Yamini

Shamsayei

2021

J of Separation Science

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Porous frameworks are a term of attracting solid materials assembled by interconnection of molecules and ions. These trendy materials due to high chemical and thermal stability, well-defined pore size and structure, and high effective surface area gained attention to employ as extraction phase in sample pretreatment methods before analytical analysis. Solid-phase microextraction is an important subclass of sample preparation technique that up to now different configurations of this method have been introduced to get adaptable with different environments and analytical instruments. In this review, theoretical aspect and different modes of solid-phase microextraction method are investigated. Different classes of porous frameworks and their applications as extraction phase in the proposed microextraction method are evaluated. Types and features of supporting substrates and coating procedures of porous frameworks on them are reviewed. At the end, the prospective and the challenges ahead in this field are discussed.

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Section: Applications Of Porous Framework In Microextraction Techniquesmentioning

confidence: 99%

Section: Applications Of Porous Framework In Microextraction Techniquesmentioning

confidence: 99%

mentioning

confidence: 99%

mentioning

confidence: 99%

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Applications of porous frameworks in solid‐phase microextraction

Khataei

Yamini

Shamsayei

2021

J of Separation Science

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“…Currently, the contamination of PAHs in soil is moving toward increasing severity, and therefore the detection methods for PAHs in soil are being widely studied worldwide. 16 The traditional analytical methods for laboratory detection of PAHs in soil are mainly based on chromatography, which is an effective separation and analysis technique that separates and analyzes substances based on the difference in partition coefficients between the stationary and mobile phases. Gas chromatography (GC), gas chromatography-mass spectrometry (GC-MS) and high performance liquid chromatography (HPLC) have been widely used for the detection of PAHs in soil.…”

Section: Introductionmentioning

confidence: 99%