2006
DOI: 10.1557/jmr.2006.0197
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Contact creep compliance of viscoelastic materials via nanoindentation

Abstract: The creep compliance of viscoelastic materials such as synthetic polymers is an established metric of the rate at which strain increases for a constant applied stress and can, in principle, be implemented at the nanoscale to compare quantitatively bulk or thin film polymers of different structures or processing histories. Here, we outline the evolution of contact creep compliance analysis and application for both conical and spherical indenter geometries. Through systematic experiments on four amorphous (glass… Show more

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Cited by 192 publications
(98 citation statements)
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“…Jazouli et al [16] studied the nonlinear creep behavior of polycarbonate (PC) via uniaxial tensile creep tests at different stress levels and found that the creep compliance increases with the applied stress. Tweedie et al [9] observed that the assumption of linear viscoelasticity breaks down for several polymers (including polycarbonate and polypropylene) when creep compliance is measured via conical indentation. Oyen [17] discussed the geometrical nonlinearity and material nonlinearity for indentation of nonlinear viscoelastic solids.…”
Section: Introductionmentioning
confidence: 99%
“…Jazouli et al [16] studied the nonlinear creep behavior of polycarbonate (PC) via uniaxial tensile creep tests at different stress levels and found that the creep compliance increases with the applied stress. Tweedie et al [9] observed that the assumption of linear viscoelasticity breaks down for several polymers (including polycarbonate and polypropylene) when creep compliance is measured via conical indentation. Oyen [17] discussed the geometrical nonlinearity and material nonlinearity for indentation of nonlinear viscoelastic solids.…”
Section: Introductionmentioning
confidence: 99%
“…7). This is significantly lower than the thermal drift of other instruments 19 where corrections of the thermal drift must be done numerically based on thermal drift values obtained either before or after the indentation.…”
Section: Fig 4 Fused Silica Measurements At (A) 100mentioning
confidence: 87%
“…The indenter tip penetration depth is measured during loading and unloading with a parallel plate capacitor that has sub-nanometer resolution [13]. The most common indenters include the three-sided pyramid (Berkovich) indenter, spherical indenter [14] and the flat-ended (punch) indenter [15]. The Berkovich indenter was successfully used for extracting the mechanical characteristics of individual microstructural phases in the cement paste [16].…”
Section: Nanoindentationmentioning
confidence: 99%