Abstract-Structural, vibrational and microwave dielectric properties of Nickel-Copper-Zinc ferrite (Ni 0.2 Cu x Zn 0.8−x Fe 2 O 4 ) ceramics have been presented in this paper. Samples have been prepared using conventional auto-combustion method. The X-ray diffraction (XRD) results confirmed the ferrite samples to be of cubic spinel structure, which further was validated by Fourier transform infrared (FT-IR) and Raman spectroscopy. The relative permittivity (ε r ) increased from 7.474 to 8.132 with successive increase in Cu content. The observed and calculated permittivity using ClausiusMossoitti relation have been in good agreement. The temperature coefficient of resonant frequency (τ f ) decreased from −75.85 ppm/ • C to −32.12 ppm/ • C with increase in successive Cu content. The relative permeability (µ r ) have been calculated by using the Nicholson-Ross-Weir conversion technique. Using Ni 0.2 Cu 0.2 Zn 0.6 Fe 2 O 4 sample the ferrite resonator antennas have been designed in three different shapes. The experimental and theoretical characteristics of the antennas have been compared and a good agreement has been achieved.