Compound Radiofrequency-Driven Recoupling Pulse Sequences for Efficient Magnetization Transfer by Homonuclear Dipolar Interaction under Magic-Angle Spinning Conditions

Accurate measurement of C13–N15 distances with solid-state NMR

“…MAS also averages the dipole-dipole couplings, and they should be reintroduced by using a rotational resonance. 10 Rotor-synchronized recoupling sequences 11 make it possible to combine sites assignment with information about dipolar couplings. When the pairs of rare nuclei are created by specific isotope labeling and, therefore, the problem of assignment is solved, the most popular techniques for measuring inter-nuclear distances under MAS are REDOR 12 (for heteronuclear pairs) and build-up of the double-quantum coherence 13 (for homonuclear pairs).…”

Assembly of a Mixture of Isomeric BChl c from Chlorobium limicola As Determined by Intermolecular 13C−13C Dipolar Correlations: Coexistence of Dimer-Based and Pseudo-Monomer-Based Stackings

“…We appreciate the other reviewer for encouraging us to mention the relevance of this solidstate aggregate of BChl c to chlorosomes.7584 Biochemistry, Vol. 45, No 24,. 2006 Kakitani et al…”

1H–13C INEPT MAS NMR correlation experiments with 1H–1H mediated magnetization exchange to probe organization in lipid biomembranes

“…This decay results from the distribution of the magnetization under RFDR via the recoupled dipolar interactions, but also can be ascribed to a non-recoverable loss of magnetization due to pulse error and timing errors in the multiple-p RFDR pulse train. The performance of the RFDR sequence may be improved by incorporation of additional RFDR phase cycling [54], or the introduction of compensated RFDR sequences [55]. For the NOE based cross-relaxation the buildup rates of the 1 H-1 H exchange is generally slower (Fig.…”