The data were obtained on the content of organic carbon in the water, particulate matter, and bot tom sediments of the Cai River and its tributaries (the basin of Nha Trang Bay). The surface waters of the con sidered basin contained OM mainly in a dissolved form (DOC/POC = 3). The fraction of C org in particulate matter amounted to 4.9% on average. Based on the analysis of n alkanes in bottom sediments, three OM types-autochthonous, mixed, and mainly terrigenous genesis-were distinguished. These types are alter nated in series in the lengthwise profile of the river. All the OM types are in close relation to the peculiarities of sedimentation and hydrodynamics of the waters in the treated aquatic area. The geochemical indices (Pr/Ph, , and CPI values) represent the influence of oxidative conditions on OM formation and the intense microbiological transformation of its autochthonous component.