Combustion synthesis of Si-related crystalline nanostructures

Soszyński, Michał; Łabędź, Olga; Huczko, A.

doi:10.1016/j.jcrysgro.2014.01.054

Cited by 7 publications

(5 citation statements)

References 17 publications

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“…In addition, a small discrepancy of the SiC content was detected when compared to the predicted ones. This research had concluded that composite (i.e SiC-Si3N4) in the Si-C-N system with controlled morphology and high purity could be attained using SHS without inert solution [16].…”

Section: Synthesize Methodsmentioning

confidence: 99%

Silicon carbide- from synthesis to application: a review

2017

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Abstract. This paper provides a review of the synthesis techniques that are used to produce nanostructured silicon carbide. The synthesis methods, consisting of carbothermal reduction, chemical vapor deposition, laser ablation, sol-gel and microwave heating are described. The silicon carbide properties and application are also explained. The paper then discusses the limitations of previous studies which involved complicated equipment and processes, that limit their further application and act as a barrier to further research and development in many fields.

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Section: Synthesize Methodsmentioning

confidence: 99%

Silicon carbide- from synthesis to application: a review

2017

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“…Thus, the CS processes have become an important tool in the synthesis of new inorganic materials . As an example, we showed elsewhere that SiC nanowires can be efficiently produced from the mixture of simple reactants (Si/Teflon ® ). Here, we aim at the CS formation of novel graphene‐related nanocarbons which have a unique variety of properties, which make them promising candidates for various applications.…”

Section: Introductionmentioning

confidence: 99%

Self‐propagating high‐temperature fast reduction of magnesium oxalate to novel nanocarbons

Huczko

Kurcz

Dąbrowska

et al. 2016

Physica Status Solidi (b)

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Phone: þ48 22 55 26 416, Fax: þ48 22 822 59 96Combustion synthesis is known as a cost-effective technique to produce many novel ceramic nanomaterials such as nitrides, carbides, and intermetallic compounds. Herein, we report an extremely fast chemical transformation of magnesium-magnesium oxalate (Mg/MgC 2 O 4 ) mixtures into solid products containing different nanocarbons and MgO. Despite a wide range of molar ratios of reactants all combustions, carried out in Ar at 1 MPa, were successful. The solid products were chemically purified (leaching of unreacted Mg and MgO) and characterized by XRD, SEM/EDX, TEM, DSC, and Raman spectroscopy. The residue contained mostly layered (circa several nm thick) carbon petal-like nanostructures and carbon-coated MgO.

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“…In recent reports, microwave heating at 1200 C of suitable mixtures of silicon, graphite, and aluminum powders yielded either α-SiC [17] or aluminum-doped β-SiC [18]. Pure or boron-doped β-SiC powders were also produced by various combustion synthesis methods [19][20][21][22][23].…”

Section: Introductionmentioning

confidence: 99%