Circular of the Bureau of Standards no. 539 volume 1:

Swanson, Howard E

doi:10.6028/nbs.circ.539v1

Cited by 64 publications

(74 citation statements)

References 43 publications

(56 reference statements)

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“…8), in agreement with the standard data [44]. In addition, the patterns inevitably comprise peaks from the Au layer, which is always present in the consequence of sample synthesis.…”

Section: Microstructure Of the Nickel Polycrystalline Frameworksupporting

confidence: 72%

Periodic order and defects in Ni-based inverse opal-like crystals on the mesoscopic and atomic scale

et al. 2014

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The structure of inverse opal crystals based on nickel was probed on the mesoscopic and atomic levels by a set of complementary techniques such as scanning electron microscopy and synchrotron microradian and wide-angle diffraction. The microradian diffraction revealed the mesoscopic-scale face-centered-cubic (fcc) ordering of spherical voids in the inverse opal-like structure with unit cell dimension of 750 ± 10 nm. The diffuse scattering data were used to map defects in the fcc structure as a function of the number of layers in the Ni inverse opal-like structure. The average lateral size of mesoscopic domains is found to be independent of the number of layers. 3D reconstruction of the reciprocal space for the inverse opal crystals with different thickness provided an indirect study of original opal templates in a depth-resolved way. The microstructure and thermal response of the framework of the porous inverse opal crystal was examined using wide-angle powder x-ray diffraction. This artificial porous structure is built from nickel crystallites possessing stacking faults and dislocations peculiar for the nickel thin films.

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“…8), in agreement with the standard data [44]. In addition, the patterns inevitably comprise peaks from the Au layer, which is always present in the consequence of sample synthesis.…”

Section: Microstructure Of the Nickel Polycrystalline Frameworksupporting

confidence: 72%

Periodic order and defects in Ni-based inverse opal-like crystals on the mesoscopic and atomic scale

et al. 2014

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“…Triangles mark reference positions for TiC (filled) and Pt (open). [30,31] There is less intensity from the as-deposited sample than in Figure 2 due to thinner coating and hence smaller diffraction volume.…”

Section: Resultsmentioning

confidence: 99%

“…This observation is general for the case of solid solution carbides of strong and weak carbide formers [12,13,15,17]. [30,31]. Table 1 Lattice parameters (a) and grain sizes (t) determined from GIXRD.…”

Section: Resultsmentioning

confidence: 99%

Carbide and nanocomposite thin films in the Ti–Pt–C system

Lewin

Buchholt

et al. 2010

Thin Solid Films

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Thin films in the Ti-Pt-C system were deposited by non-reactive, DC-magnetron sputtering.Samples were characterised using X-ray photoelectron spectroscopy, X-ray diffraction, and transmission electron microscopy. A previously not reported metastable solid solution carbide, (Ti 1-x Pt x )C y with a Pt/Ti ratio of up to 0.43 was observed. This solid solution phase was present both as single phase in polycrystalline samples, and together with amorphous carbon (a-C) in nanocomposite samples. Annealing of nanocomposite samples lead to decomposition of the solid solution phase and formation of a nc-TiC x /a-C/nc-Pt nanocomposite. Test sensors for automotive gas exhausts manufactured from such a three-phase material suffers from complete oxidation of the coating at 400 °C with no observed sensor activity.

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“…The peaks between 30 and 90 cleg have been identified as belonging to zinc oxide [5]. The peaks occurring between 6 and 26 deg are the res ul t of chemical reac tion.…”

Section: Resultsmentioning

confidence: 99%

Setting reaction of zinc oxide and eugenol

Copeland¹,

Bräuer²,

Sweeney³

et al. 1955

J. RES. NATL. BUR. STAN.

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Zinc oxide-eugenol mixt ures have bee n used in dentistry for a number of years. The setting m echanism of these mixtures was investigated. X-rav diffraction dat a and electron photomicrovaphs g ive ~vid~n ce that a crystll:lline compound is formed. Analysis and molecular-weight dettrml.nat lons show t hat th,s compound corresponds t o the empirical formula (OIOH l.' O2) 2 Zn, ztn C euge nolate. Infrared data, as well as t he nonreactivity of meta and I?ara substituted phe nols as compared to the ortho isomers, suggest that t he zinc e ugenolate IS a chelate. The hardened mass consists of zinc oxide e mbedded in a matrix of long sheath-like crystals of zin c eugenolate. The excess eugenol is sorbed by bot h t he zinc e ugenolate and the zinc oxide.

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Circular of the Bureau of Standards no. 539 volume 1:

Cited by 64 publications

References 43 publications

Periodic order and defects in Ni-based inverse opal-like crystals on the mesoscopic and atomic scale

Periodic order and defects in Ni-based inverse opal-like crystals on the mesoscopic and atomic scale

Carbide and nanocomposite thin films in the Ti–Pt–C system

Setting reaction of zinc oxide and eugenol

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