ChemInform Abstract: SYNTHESIS AND STRUCTURE OF 2‐AMINOOXAZOLINE DERIVATIVES

Tsoi, L. A.; Salimbaeva, A. D.; Abiyurov, B. D.

doi:10.1002/chin.198414207

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2007

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“…Phenylphosphoric acid was purchased from TCI Europe. 1-Allyl-3-phenylurea (4) [45] and 1-allyl-3-(phenyl)thiourea (7) [46] were synthesised following reported procedures.…”

Section: Methodsmentioning

confidence: 99%

Phenylphosphoric Acid as a New Additive to Inhibit Olefin Isomerisation in Ruthenium‐Catalysed Metathesis Reactions

et al. 2007

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A systematic study of the ruthenium-catalysed metathesis of alkenes containing hydrogen-bonding substituents (namely urea and thiourea groups) is presented. Under standard metathesis conditions, several of the substrates under study undergo alkene isomerisation instead of the targeted metathesis. However, in the course of these investigations it has been established that this unwanted isomerisation process can be suppressed by addition of phenylphosphoric acid to the reaction mixture. Some other potential isomerisation inhibitors (e.g. benzoic acid and salts of phosphoric acid) have been

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“…Phenylphosphoric acid was purchased from TCI Europe. 1-Allyl-3-phenylurea (4) [45] and 1-allyl-3-(phenyl)thiourea (7) [46] were synthesised following reported procedures.…”

Section: Methodsmentioning

confidence: 99%