ChemInform Abstract: Syngas‐Mediated C—C Bond Formation in Flow: Selective Rhodium‐Catalyzed Hydroformylation of Styrenes.

Kasinathan, Sivarajan; Bourne, Samuel L.; Tolstoy, Paeivi; Koóš, Peter; O’Brien, Matthew; Bates, Roderick W.; Baxendale, Ian R.; Ley, Steven V.

doi:10.1002/chin.201213080

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2016

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“…A Teflon semipermeable membrane allowed the controlled addition of CO, thus improving selectivity and safety [40]. A tube-in-tube reactor was also used for the idroformylation of styrenes with syngas [41]. The dual concept has been proposed by Gutmann et al [42], suggesting to shift the equilibrium of aldehydes decarbonilation by removing selectively CO in a tube-in-tube reactor.…”

Section: Methodsmentioning

confidence: 99%

Chemical reaction engineering, process design and scale-up issues at the frontier of synthesis: Flow chemistry

Rossetti

Compagnoni

2016

Chemical Engineering Journal

202

103

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Flow chemistry has been proposed in modern organic chemistry as a mean for process intensification, to improve the control over reaction performance and to achieve higher yield. However, many open issues can be evidenced regarding the true possibility of scale-up, as well as currently lacking information for process design and economical evaluation. This review proposes some recent examples of flow synthesis deepening in particular the scale-up and engineering issues. Required information is evidenced, as well as some transport and kinetic data required for the practical implementation of the results.

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Section: Methodsmentioning

confidence: 99%