ChemInform
 1987
DOI: 10.1002/chin.198704227
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ChemInform Abstract: Cleavage of Phosphorus‐Carbon Bonds with Sodium/Naphthalene. Facile Preparation of Unsymmetrical Diphosphines.

Ta Shue Chou1,
Chung-Huang Tsao2,
Su Chun Hung3

Abstract: The bis(diphenylphosphino)alkanes (I) react with sodium/naphthalene under reductive cleavage of the aryl‐phosphorus bond to yield the compound (II) which can be methylated to (III).

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