Chemical Processes in Marine Environments

Gianguzza, Antonio; Pelizzetti, Ezio; Sammartano, Silvio

doi:10.1007/978-3-662-04207-6

2000

DOI: 10.1007/978-3-662-04207-6

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Chemical Processes in Marine Environments

Antonio Gianguzza¹,

Ezio Pelizzetti²,

Silvio Sammartano³

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Cited by 8 publications

References 388 publications

(563 reference statements)

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Ultra‐high performance supercritical fluid chromatography of lignin‐derived phenols from alkaline cupric oxide oxidation

Sun

Lidén

Sandahl

et al. 2016

J of Separation Science

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Traditional chromatographic methods for the analysis of lignin‐derived phenolic compounds in environmental samples are generally time consuming. In this work, an ultra‐high performance supercritical fluid chromatography method with a diode array detector for the analysis of major lignin‐derived phenolic compounds produced by alkaline cupric oxide oxidation was developed. In an analysis of a collection of 11 representative monomeric lignin phenolic compounds, all compounds were clearly separated within 6 min with excellent peak shapes, with a limit of detection of 0.5–2.5 μM, a limit of quantification of 2.5–5.0 μM, and a dynamic range of 5.0–2.0 mM (R 2 > 0.997). The new ultra‐high performance supercritical fluid chromatography method was also applied for the qualitative and quantitative analysis of lignin‐derived phenolic compounds obtained upon alkaline cupric oxide oxidation of a commercial humic acid. Ten out of the previous eleven model compounds could be quantified in the oxidized humic acid sample. The high separation power and short analysis time obtained demonstrate for the first time that supercritical fluid chromatography is a fast and reliable technique for the analysis of lignin‐derived phenols in complex environmental samples.

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Ultra‐high performance supercritical fluid chromatography of lignin‐derived phenols from alkaline cupric oxide oxidation

Sun

Lidén

Sandahl

et al. 2016

J of Separation Science

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Cr(III)/Cr(VI) speciation determination of chromium in water samples by luminescence quenching of quercetin

Hosseini

Belador

2009

Journal of Hazardous Materials

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Formation and stability of mixed Mg2+/Ca2+/phytate species in synthetic seawater media

et al. 2008

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Chemical Processes in Marine Environments

Cited by 8 publications

References 388 publications

Ultra‐high performance supercritical fluid chromatography of lignin‐derived phenols from alkaline cupric oxide oxidation

Ultra‐high performance supercritical fluid chromatography of lignin‐derived phenols from alkaline cupric oxide oxidation

Cr(III)/Cr(VI) speciation determination of chromium in water samples by luminescence quenching of quercetin

Formation and stability of mixed Mg2+/Ca2+/phytate species in synthetic seawater media

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