“…Fractions F9–F14 (991 mg), in which the antifungal activity was concentrated, were purified by semipreparative HPLC: sample (80 mg/mL, total volume 2.5 mL), Luna C 18 column (250 mm × 21.20 mm i.d., 10 μm), with a gradient elution by CH 3 CN–H 2 O–MeOH (5% CH 3 CN in 5 min, 40% CH 3 CN in 60 min, purge 100% MeOH in 65 min, and 5% CH 3 CN in 175 min), a flow rate of 10 mL/min, injection volume of 500 μL, detection at 320 nm, to afford forsythoside A ( 3 , t R 8.69 min), verbascoside ( 4 , t R 8.95 min), and isoverbascoside ( 5 , t R 9.43 min) . From fractions F16 (77 mg) and F18 (35 mg), yellow solids precipitated (30 and 7 mg, respectively), which were identified as pectolinarin ( 7 ) and linarin ( 8 ) …”