Chemical attribution of the homemade explosive ETN - Part II: Isotope ratio mass spectrometry analysis of ETN and its precursors

Bezemer, Karlijn; McLennan, Lindsay; Hessels, Rosanne; Schoorl, Jorien; Elshout, Jos van den; Heijden, Antoine van der; Hulsbergen, Annemieke; Koeberg, Mattijs; Busby, Taylor; Yevdokimov, Alexander; Rijke, Eva de; Schoenmakers, Peter J.; Smith, James L.; Oxley, Jimmie C.; Asten, Arian C. van

doi:10.1016/j.forsciint.2020.110344

Cited by 15 publications

(5 citation statements)

References 22 publications

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“…Comparison of the homemade explosive erythritol tetranitrate (ETN) with its precursors was explored in a paper published by Bezemer, K et al Keying in on carbon and nitrogen they report that “… robust linear relationships between precursor and the end product were observed for these isotopes … that support the hypothesis that a given erythritol or nitrate precursor was used to synthesis a specific ETN batch.” [ 488 ].…”

Section: Instrumental Analysis Of Explosivesmentioning

confidence: 99%

Interpol review of the analysis and detection of explosives and explosives residues

Klapec

Czarnopys

Pannuto

2023

Forensic Science International: Synergy

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Section: Instrumental Analysis Of Explosivesmentioning

confidence: 99%

Interpol review of the analysis and detection of explosives and explosives residues

Klapec

Czarnopys

Pannuto

2023

Forensic Science International: Synergy

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“…Intrinsic markers are studied by using isotope ratios using nuclear magnetic resonance spectroscopy (NMR) or isotope ratio mass spectrometry (IRMS). IRMS has been used for instance when links between precursor and home-made explosives were investigated [43]. NMR analysis using carbon 13 isotope ratios has been used in a study of methylphosphonic dichloride (DC) [44].…”

Section: Chemical Attribution Signatures In Cwasmentioning

confidence: 99%

Route attribution of chemical warfare agents : Retrospective classification of unknown threat samples

Holmgren

2022

Linköping Studies in Science and Technology. Dissertations

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respectively. All participating laboratories analysed the same samples prepared at the Swedish Defence Research Agency (FOI). The impurity profiles in nerve agent precursor metylphosphonyl dichloride samples were compared by a gas chromatography mass spectrometry (GC/MS) method using a retention index to facilitate data comparison. Retention indices of 16 CASs were calculated and compared, and this showed that the between-laboratory variation was low. This work is a first step towards a harmonised laboratory method for the profiling of CWA samples. The methods developed in this thesis will enhance accurate source attribution of CWAs and could potentially be used when alleged use of a CWA is being investigated.

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“…O principal interesse de grupos terroristas pelo ETN se deve à acessibilidade ao precursor de síntese eritritol, comercialmente disponível como um adoçante de baixo valor calórico. Assim, foi considerado pelas autoridades de diversos países como explosivo caseiro para futuras ações terroristas (MANNER, PRESTON, et al, 2015;LEASE, KAY, et al, 2019;BEZEMER, MCLENNAN, et al, 2020b;FREYE, KINMAN, et al, 2020).…”

Section: Figura 3 -Fórmulas Estruturais: (A) Etn (B) Ng E (C) Petnunclassified

Revista Susp 2° Edição

2022

Revista Susp

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Periódico semestral interdisciplinar do Ministério da Justiça e Segurança Pública, que busca disseminar o conhecimento científico, técnico e profissional na área da Segurança Pública, com vistas a contribuir com a ampliação e consolidação de boas práticas e com o compartilhamento de experiências para desenvolvimento científico, a formação e o aperfeiçoamento de profissionais integrantes do Sistema Único de Segurança Pública (Susp). A revista publica artigos originais, revisão de literatura, relatos de experiências, notas técnicas, resenhas, críticas científicas, traduções e entrevistas, publicados em formato impresso e eletrônico. COMITÊ CIENTÍFICO

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Chemical attribution of the homemade explosive ETN - Part II: Isotope ratio mass spectrometry analysis of ETN and its precursors

Cited by 15 publications

References 22 publications

Interpol review of the analysis and detection of explosives and explosives residues

Interpol review of the analysis and detection of explosives and explosives residues

Route attribution of chemical warfare agents : Retrospective classification of unknown threat samples

Revista Susp 2° Edição

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