2019
DOI: 10.1186/s40494-019-0279-5
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Characterization of the residues in Han Dynasty bronze lamps by pyrolysis–gas chromatography–mass spectrometry

Abstract: The fuel residues in two bronze lamps excavated from Haihunhou Tomb in the Han Dynasty, in Jiangxi Province, China, were studied in this paper. The techniques of Fourier transform infrared (FT-IR) spectroscopy and pyrolysis-gas chromatography-mass spectrometry with thermal-assisted hydrolysis and methylation (THM-Py-GC/MS) were used to characterize the materials. Long-chain fatty acids, fatty alcohols and hydrocarbons were detected as the main components. By comparing the reference materials of beeswax and Chi… Show more

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Cited by 7 publications
(2 citation statements)
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“…Gas chromatography-mass spectrometry (GC-MS) is widely used to separate and detect organic residues: Laura Blanco-Zubiaguirre analysis the wine markers in archeological potteries at ultratrace levels, [7] Shuya Wei analysis the lamp oil residue from Haihunhou Tomb. [8] Joanna Kałuż na-Czaplińska reviews the analytical procedures of different organic residue (lipids, fatty acids and other biomarkers) based on the GC-MS. However, traditional quadrupole instruments provide limited sensitivity in the scan mode.…”
Section: Introductionmentioning
confidence: 99%
“…Gas chromatography-mass spectrometry (GC-MS) is widely used to separate and detect organic residues: Laura Blanco-Zubiaguirre analysis the wine markers in archeological potteries at ultratrace levels, [7] Shuya Wei analysis the lamp oil residue from Haihunhou Tomb. [8] Joanna Kałuż na-Czaplińska reviews the analytical procedures of different organic residue (lipids, fatty acids and other biomarkers) based on the GC-MS. However, traditional quadrupole instruments provide limited sensitivity in the scan mode.…”
Section: Introductionmentioning
confidence: 99%
“…In addition to the merits listed above, what amazed people most is the environmentally friendly design concept demonstrated by this artifact. It is widely believed that when the lamp was used for lighting 2,000 y ago, the goose belly was filled with water and the long neck served as a duct for the smoke generated by burning plant oil, animal fat, or wax ( 4 ). Rather than polluting the indoor air, the smoke flowed into the belly through the neck and was finally absorbed by the water.…”
mentioning
confidence: 99%