Characterization of the Microstructure, Local Macro-Texture and Residual Stress Field of Commercially Pure Titanium Grade 2 Prepared by CONFORM ECAP

Abstract

The paper investigated the residual strain and stress distribution, microstructure, and macro-texture along the transverse direction of commercially pure titanium grade 2 samples prepared by the CONFORM ECAP technique. This method belongs to the severe plastic deformation methods; hence, it could be assumed that residual stress fields would be present in the work-pieces. Residual stresses cannot be directly measured; thus, neutron diffraction measurements, Electron back-scatter diffraction (EBSD) investigations, and local X-ray macro-texture measurements were performed in different regions of the sample to determine the data for the residual stress calculation. The calculation was based on the modified Kröner model. Neutron diffraction strain scans and residual stress calculations revealed that symmetrical residual strain and stress gradients with compression character were present in the axial and hoop direction after one and two passes. Asymmetric distribution of the residual strains and stresses remained after the third pass of the CONFORM ECAP. EBSD investigations showed that after the first pass, significant grain refinement occurred; however, further passes did not cause any dramatic grain refinement. X-ray texture measurements revealed that local macro-texture was dependent on the number of passes of the CONFORM ECAP and on the investigated area in the samples.

Optimization of the Mechanical Performance of Titanium for Biomedical Applications by Advanced, High-Gain SPD Technology

“…Evidence for mechanical twinning was not found by EBSD investigation. The same results were found in our previous studies [16,37] on Conform SPD-ed titanium Grade 2. After Conform SPD and rotary swaging process, both materials exhibited fibre texture and the prismatic (101 0) planes were perpendicular to the processing direction.…”