“…This second one turned out to be preferable as samples did not require any particular preparation prior to observations, whereas, in case of the high-vacuum instrument, carbon coating was required to render the samples electrically conductive and, therefore, better observable. Observation conditions, like magnification, accelerating voltage (20 KeV for our tests), beam current, etc., were selected following standard recommendations and the specific requirements deriving from the actual microstructure of each sample [32][33][34]. Both microscopes were equipped with an EDXS system, used to evaluate compositions of the observed regions.…”