Characterization of a novel natural cellulosic fiber extracted from the stem of Chrysanthemum morifolium

Dalmış, Ramazan; Kılıç, Gonca Balcı; Seki, Yasushi; Köktaş, Serhan; Keskin, Özgür Yasin

doi:10.1007/s10570-020-03385-2

Cited by 59 publications

(45 citation statements)

References 81 publications

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“…For the cellulose standard, besides the peak at 897 cm −1 , we observed another one at 876 cm −1 that was not present in the stems of the four species analyzed (Figure 5). The peak situated in this region (≈890 cm −1 ) was attributed to glycosidic bonds of monosaccharides [3,[53][54][55][56] as well as to the amorphous region of cellulose [40]. Similarly, in Abutilon indicum lignocellulosic fibers, a peak around 899 cm −1 was identified and attributed to the vibration of functional group C-O-C [10].…”

Section: Resultsmentioning

confidence: 92%

Comparative FT-IR Prospecting for Cellulose in Stems of Some Fiber Plants: Flax, Velvet Leaf, Hemp and Jute

et al. 2021

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Plant fibers are sustainable sources of materials for many industries, and can be obtained from a variety of plants. Cellulose is the main constituent of plant-based fibers, and its properties give the characteristics of the fibers obtained. Detailed characterization of cellulosic fibers is often performed after lengthy extraction procedures, while fast screening might bring the benefit of quick qualitative assessment of unprocessed stems. The aim of this research was to define some marker spectral regions that could serve for fast, preliminary qualitative characterization of unprocessed stems from some textile plants through a practical and minimally invasive method without lengthy extraction procedures. This could serve as a screening method for sorting raw materials by providing an accurate overall fingerprint of chemical composition. For this purpose, we conducted comparative Fourier Transform Infrared Spectroscopy (FT-IR) prospecting for quality markers in stems of flax (Linum usitatissimum L.), velvet leaf (Abutilon theophrasti Medik.), hemp (Cannabis sativa L.) and jute (Corchorus olitorius L.). Analysis confirmed the presence of major components in the stems of the studied plants. Fingerprint regions for cellulose signals were attributed to bands at 1420–1428 cm−1 assigned to the crystalline region and 896–898 cm−1 assigned to the amorphous region of cellulose. The optimization of characterization methods for raw materials is important and can find immediate practical applications.

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Section: Resultsmentioning

confidence: 92%

Comparative FT-IR Prospecting for Cellulose in Stems of Some Fiber Plants: Flax, Velvet Leaf, Hemp and Jute

et al. 2021

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“…The relative surface composition of rattan fiber is 63.44% C, 31.08% O, 1.64% N and 3.85% Si. O/C ratio of rattan fiber is obtained as 0.49, which is higher than many other mostly utilized lignocellulosic fibers such as Linden (0.13) (Seki et al 2014), Conium maculatum (0.21) (Kılınç et al 2018), Henequen (0.25) (Sgriccia et al 2008), hemp (0.27) (Sgriccia et al 2008), Chrysanthemum morifolium (0.41) (Dalmis et al 2020), Kenaf (0.45) (Sgriccia et al 2008) and Hierochloe Odarata (0.48) (Dalmis et al 2019). However, the value is lower than that of Luffa cylindrica (0.61) (Seki et al 2013) and oil palm mesocarp fiber (1.00).…”

Section: Xps Analysismentioning

confidence: 82%

“…The wavenumber at 1050 cm -1 manifests the existence of C-O groups of cellulose (Manimaran et al 2018). The peak around 897 cm -1 is associated with the β-glycosidic linkages between the monosaccharides (Dalmis et al 2020). The little peak located at 604 cm -1 represents the C-OH bending (De Rosa et al 2010).…”

Section: Ftir Analysismentioning

confidence: 99%

“…A peak detected at 1376 cm -1 is attributed to C-H groups of cellulose (Belouadah et al 2015). Vibration peak of 1246 cm -1 means C-O stretching vibration of the acetyl groups in lignin (Dalmis et al 2020). The peak at 1164 cm -1 is ascribed to C-O-C groups of cellulose and hemicellulose (De Rosa et al 2010).…”

Section: Ftir Analysismentioning

confidence: 99%

“…Recently, on account of the increasing demand for plant fibers in industry, researchers have sought and studied new natural fibers such as Heteropogon Contortus (Hyness et al 2017), Conium maculatum (Kılınç et al 2018), Catharanthus roseus (Vinod et al 2019), Thespesia populnea (Kathirselvam et al 2019b), Chrysanthemum morifolium (Dalmis et al 2020), Hierochloe Odarata (Dalmis et al 2019).…”

Section: Introductionmentioning

confidence: 99%

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Characterization of novel natural fiber from manau rattan (Calamus manan) as a potential reinforcement for polymer-based composites

Ding

Han

et al. 2021

Preprint

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The study on novel natural fibers in polymer-based composites will help promote the invention of novel reinforcement and expand their possible applications. Herein, novel cellulosic fibers were extracted from the stem of manau rattan (Calamus manan) by mechanical separation. It is the first time to comprehensively analyze and study the chemical, thermal, mechanical and morphological properties of manau rattan fibers by Fourier Transform Infrared Spectroscopy (FTIR), X-Ray Photoelectron Spectroscopy (XPS), X-Ray Diffraction Analysis (XRD), Thermogravimetric Analysis (TGA), single fiber tensile test and Scanning Electron Microscopy (SEM). Component analysis results showed the cellulose, hemicellulose and lignin contents of manau rattan fibers were 42, 20, and 27%, respectively. The surface of the rattan fiber was hydrophilic according to the oxygen/carbon ratio of 0.49. Manau rattan has a high crystalline index of 48.28%, inducing a high maximum degradation temperature of 332.8°C. This reveals that it can be used as a reinforcement for thermoplastic composites whose operating temperature is below 300°C. The average tensile strength can reach 273.28 MPa, which is beneficial to improve the mechanical properties of rattan fiber reinforced composites. SEM images displayed the rough surface of the fiber, which helps to enhance the interfacial adhesion between the fibers and matrices in composites. This work was also in comparison with some other natural fibers. The above analysis and research showed the great potential of manau rattan fibers as the reinforcement in polymer-based composites.

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Study on the characteristics of novel natural fiber extracted from Coccinia grandis plant vine: a novel material for engineering applications

Raja,

Ali,

Shashi Kumar

et al. 2024

Int J Adv Manuf Technol

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Characterization of a novel natural cellulosic fiber extracted from the stem of Chrysanthemum morifolium

Cited by 59 publications

References 81 publications

Comparative FT-IR Prospecting for Cellulose in Stems of Some Fiber Plants: Flax, Velvet Leaf, Hemp and Jute

Comparative FT-IR Prospecting for Cellulose in Stems of Some Fiber Plants: Flax, Velvet Leaf, Hemp and Jute

Characterization of novel natural fiber from manau rattan (Calamus manan) as a potential reinforcement for polymer-based composites

Study on the characteristics of novel natural fiber extracted from Coccinia grandis plant vine: a novel material for engineering applications

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