Abstract:The phosphomolybdate-PAMAM nanocomposite film was successfully prepared by using a submonolayer of 3-mercaptopropionic acid (3-MPA) adsorbed on a polycrystalline gold electrode further reacted with poly(amidoamine) (PAMAM) dendrimer (generation 4.0) to obtain a film on which 1:12 phosphomolybdate acid (PMo12) was later coordinated to afford a mixed electrocatalytic layer. On the basis of the electrochemical behaviors, atomic force microscopy (AFM) and X-ray photoelectron spectra (XPS), it is suggested that the… Show more
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