2010
DOI: 10.1107/s1600536810004861
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Bis{tris[3-(2-pyridyl)-1H-pyrazole]iron(II)} dodecamolybdo(V,VI)phosphate hexahydrate

Abstract: Crystals of the title compound, [Fe(C8H7N3)3]2[PMo12O40]·6H2O, prepared under hydro­thermal conditions, are isotypic with the Mn2+ and Cd2+ analogues. The Fe2+ cation is in a distorted octa­hedral coordination by six N atoms from three chelating 3-(2-pyrid­yl)-1H-pyrazole ligands. The heteropoly­anion [PMo12O40]4− is a one-electron reduced species in which two O atoms of the central PO4 group ( symmetry) are equally disordered about an inversion centre. N—H⋯O and O—H⋯O hydrogen bonds make a contribution to the… Show more

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