Aquametric Methods in Organic Analysis.

Mitchell, J. F.

doi:10.1021/ac60217a005

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1966

2002

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Cited by 3 publications

(3 citation statements)

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“…Since tertiary hydroxyls are extremely unlikely in polyesters, the selective determination of primary and secondary hydroxyl concentrations in polyesters should be possible with TEA. Selective determinations of this type also were suggested by Mitchell in TEA esterification studies in dioxane solution (6).…”

Section: Resultsmentioning

confidence: 83%

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Aquametric determination of hydroxyl groups with trifluoroacetic acid. Application to polyesters

Lucchesi¹,

Bernstein²,

Bangasser³

1975

Anal. Chem.

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Section: Resultsmentioning

confidence: 83%

“…a NVM = Nonvolatile matter 6. Provided by the Sherwin-Williams Co. and obtained by a method similar to ASTM D1957-63.c Results of ASTM round robin for samples A-l, -2, -3, and -4.ANALYTICAL CHEMISTRY, VOL.…”

mentioning

confidence: 99%

Aquametric determination of hydroxyl groups with trifluoroacetic acid. Application to polyesters

Lucchesi¹,

Bernstein²,

Bangasser³

1975

Anal. Chem.

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“…The normal Karl Fisher technique was used by Pollio (146) to determine moisture in ion exchange resins by direct titration of the resin in methanol or pyridine. Mitchell (132) has given a survey of aquametric methods used in organic analysis.…”

Section: Methods and Applicationsmentioning

confidence: 99%

Titrations in Nonaqueous Solvents

Harlow¹,

Morman²

1966

Anal. Chem.

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A lthoughthere have been no dra-_£\_ matic "breakthroughs" during the last two years there has been notable advance in several areas. Particularly gratifying is the number of outstanding papers devoted to the fundamentals of nonaqueous equilibria. Not only are some of the more commonly used solvents such as acetonitrile receiving continued attention, but theoretical studies are being extended to solvents of very low7 dielectric constant. There appears to be a trend toward utilizing the newer types of measurements such as nuclear magnetic resonance and toward using several different types of measurements in the same investigation. In some of the recent work, for example, one finds spectrophotometric, conductometric, potentiometric, and solubility measurements combined to achieve an understanding not possible with a single technique. In the area of study concerned with the effect of solvent and acid structure on acidity, new and imaginative ideas have been introduced.

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