Aqua(1,10-phenanthroline-κ²N,N′)(pyridine-2,6-dicarboxylato-κ³N,O,O′)nickel(II) monohydrate

Abstract

Key indicatorsSingle-crystal X-ray study T = 293 K Mean (C-C) = 0.004 Å R factor = 0.034 wR factor = 0.081 Data-to-parameter ratio = 15.4For details of how these key indicators were automatically derived from the article, see

(Pyridine-2,6-dicarboxylato-κ3 O,N,O′)(2,2′:6′,2′′- terpyridine-κ3 N,N′,N′′)nickel(II) dimethylformamide monosolvate monohydrate

“…With reference to the title complex, [Ni(dipic)(terpy)]ÁC 3 H 7 NOÁH 2 O (dipic = pyridine-2,6-dicarboxylate; terpy = 2,2 0 :6 0 ,2"-terpyridine), the crystal structures of related Ni II complexes [Ni(dipic)(H 2 O) 2 ] (Liu et al, 2006), [Ni(dipic)(1,10-phenanthroline)(H 2 O)]Á-H 2 O (Ramadevi et al, 2006) and [NiCl(terpy) O (Corté s et al, 1985) have been determined previously.…”

Aqua(4-carboxypyridine-2,6-dicarboxylato-κ3O2,N,O6)(1,10-phenanthroline-κ2N,N′)nickel(II)

“…For the synthesis of pyridine-2,4,6-tricarboxylic acid, see: Syper et al (1980). For related structures, see: Ma et al (2002); Ramadevi et al (2006); Harrison et al (2006).…”