Analysis of synthetic antioxidants in salmon silage using QuEChERS extraction method followed by determination by LC-MS/MS; a single-laboratory validation study

Guldberg, Trude; Sandrød, M.; Øiaas, J.B.; Holten, Torunn; Zahlsen, Kolbjørn; Kvitvang, Hans Fredrik Nyvold

doi:10.1016/j.jchromb.2021.122715

Cited by 8 publications

(2 citation statements)

References 17 publications

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“…In another research, Guldberg et al [ 70 ] employed QuEChERS for the extraction of BHA and PG in fish silage and fish oil used to produce animal feed. This extraction was performed to develop and validate a new method to determine these antioxidants by LC–MS/MS and allowed for the quantification of antioxidants in all matrices with low detection limits of 0.012 to 0.015 mg/kg and a recovery range of 97% to 101%.…”

Section: Chemical Analysis Of Synthetic Antioxidants In Foodstuffsmentioning

confidence: 99%

Detection of Synthetic Antioxidants: What Factors Affect the Efficiency in the Chromatographic Analysis and in the Electrochemical Analysis?

Gonçalves-Filho

Souza

2022

Molecules

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Antioxidants are food additives largely employed to inhibit oxidative reactions in foodstuffs rich in oils and fat lipids, extending the shelf life of foodstuffs and inhibiting alterations in color, flavor, smell, and loss of nutritional value. However, various research has demonstrated that the inadequate use of synthetic antioxidants results in environmental and health problems due to the fact that some of these compounds present toxicity, and their presence in the human body, in high concentrations, is related to the development of some cancer types and other diseases. Therefore, the development of analytical methods for identifying and quantifying synthetic antioxidants in foodstuffs is fundamental to quality control and in ensuring consumer food safety. This review describes the recent chromatographic and electrochemical techniques used in the detection of synthetic phenolic antioxidants in foodstuffs, highlighting the main characteristics, advantages and disadvantages of these methods, and specific typical features, which include extraction methods for sample preparation and materials used in the working electrode construction, considering chromatographic and voltammetric methods, since these specific features influence the efficiency in the analysis.

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Section: Chemical Analysis Of Synthetic Antioxidants In Foodstuffsmentioning

confidence: 99%

Detection of Synthetic Antioxidants: What Factors Affect the Efficiency in the Chromatographic Analysis and in the Electrochemical Analysis?

Gonçalves-Filho

Souza

2022

Molecules

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“…70 BHA has been widely used in other daily consumer products besides food, such as petroleum feed, cosmetics, rubber and plastics. 27,[74][75][76] BHA can be detected in many environmental media due to its large carrying effect, good volatility and transferability to all environmental media 77 (Table 2). Among all reported environmental media, BHA was found at the highest levels in house dust.…”

Section: Environmental Concentrations Of Bhamentioning

confidence: 99%

A review of the occurrence, metabolites and health risks of butylated hydroxyanisole (BHA)

2023

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Butylated hydroxyanisole (BHA) is mainly used as a food additive due to its antioxidant properties, which prevent or delay oxidation reactions and extend the storage life of products. The widespread use of BHA has led to its extensive presence in various environmental matrices and human tissues. Food intake is the main route of human exposure to BHA. Under different conditions, BHA can produce different metabolites, with tert‐butyl hydroquinone (TBHQ) being one of the major products. Several studies have shown that BHA could cause thyroid system damage, metabolic and growth disorders, neurotoxicity, and carcinogenesis. Mechanisms such as endocrine disruption, genotoxicity, disturbances of energy metabolism, reactive oxygen species (ROS) production, signaling pathways, and imbalances in calcium homeostasis appear to be associated with the toxic effects of BHA. Avoiding the toxic effects of BHA to the maximum extent possible is a top priority. Finding safe, non‐toxic and environmentally friendly alternatives to BHA should be the focus of subsequent research. In all, this review summarized the current situation related to BHA and might make recommendations for future research directions. © 2023 Society of Chemical Industry.

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A green extraction strategy for the detection of antioxidants in food simulants and beverages migrated from plastic packaging materials

et al. 2023

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Analysis of synthetic antioxidants in salmon silage using QuEChERS extraction method followed by determination by LC-MS/MS; a single-laboratory validation study

Cited by 8 publications

References 17 publications

Detection of Synthetic Antioxidants: What Factors Affect the Efficiency in the Chromatographic Analysis and in the Electrochemical Analysis?

Detection of Synthetic Antioxidants: What Factors Affect the Efficiency in the Chromatographic Analysis and in the Electrochemical Analysis?

A review of the occurrence, metabolites and health risks of butylated hydroxyanisole (BHA)

A green extraction strategy for the detection of antioxidants in food simulants and beverages migrated from plastic packaging materials

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