Analysis of sulfonamides, trimethoprim, fluoroquinolones, quinolones, triphenylmethane dyes and methyltestosterone in fish and shrimp using liquid chromatography–mass spectrometry

Storey, Joseph M; Clark, Stephen Nowland; Johnson, Aaron; Andersen, Wendy C.; Turnipseed, Sherri B; Lohne, Jack J.; Burger, Robert; Ayres, Patrick R.; Carr, Justin R; Madson, Mark R.

doi:10.1016/j.jchromb.2014.09.009

Cited by 56 publications

(49 citation statements)

References 19 publications

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“…Analysis was carried out by LC-MS/MS system, separation was achieved by a YMC ODS-AQ 2ˆ100 mm, 3 µm column, and the mobile phase consisted of 0.1% formic acid in water and acetonitrile delivered under gradient elution. This method does not require a SPE cleanup step because it is fast and inexpensive, and an analytical chemist can prepare and analyze 12-16 samples per working day [83].…”

Section: Multi-residue Methodsmentioning

confidence: 99%

On the Extraction of Antibiotics from Shrimps Prior to Chromatographic Analysis

et al. 2016

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Abstract:The widespread use of antibiotics in veterinary practice and aquaculture has led to the increase of antimicrobial resistance in food-borne pathogens that may be transferred to humans. Global concern is reflected in the regulations from different agencies that have set maximum permitted residue limits on antibiotics in different food matrices of animal origin. Sensitive and selective methods are required to monitor residue levels in aquaculture species for routine regulatory analysis. Since sample preparation is the most important step, several extraction methods have been developed. In this review, we aim to summarize the trends in extraction of several antibiotics classes from shrimps and give a comparison of performance characteristics in the different approaches.

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Section: Multi-residue Methodsmentioning

confidence: 99%

On the Extraction of Antibiotics from Shrimps Prior to Chromatographic Analysis

et al. 2016

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“…Recently these applications were reviewed [9], and in particular, a review focused on using magnetic nanoparticles for the selective extraction of trace species from a complex matrix was reported [83].…”

Section: Magnetic Nanoparticle Extractionmentioning

confidence: 99%

Trends in Microextraction Techniques for Sample Preparation

2018

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“…152,153 These procedures did not include stabilizing compounds (i.e., HAH, TMPD, p-TSA) and eliminated the dichloromethane partitioning as well. Storey et al 154 developed a procedure to extract fish with McIlvaine buffer (pH 4.5), EDTA, p-TSA, and TMPD for an LC-MS/MS residue screening method without additional liquid-or solid-phase clean-up. Van de Riet et al 155 developed an extraction procedure to permit sensitive LC-MS/MS determination based on a simple tissue extraction using acetonitrile and perchloric acid, with dichloromethane and SPE clean-up.…”

Section: Procedures To Extract and Analyze Triphenylmethane Dye Residmentioning

confidence: 99%