The current study involved the calculation of air pollutant emission factors (EFs) generated from the incineration of agricultural residues. The process included sample collection, weight measurement, moisture measurement, incineration system configuration, and concentration measurement. The average CO emission factor of gaseous air pollutants from the incineration of barley and wheat agricultural residues was calculated as 0.08289 kg/kg and 0.06665 kg/kg, respectively, whereas the average NO X emission factor for barley and wheat agricultural residues was determined to be 0.00518 kg/kg and 0.00185 kg/kg, respectively. In the existing air pollutant emission calculation manual, the EF is presented only for barley. Therefore, in this study, we have introduced the EF for wheat, previously absent in the calculation manual. Additionally, the air pollutant calculation manual presents the EF of air pollutants as one value, but in this study, EF values corresponding to 2.5% and 97.5% were presented in consideration of the distribution of experimental values as shown in EMEP/EEA data.