Aldehyde—Phenol Reaction Products and Derivatives

Faith, H. Eldridge

doi:10.1021/ja01158a049

Cited by 25 publications

(5 citation statements)

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“…ce dures to give [13][14][15][16]. In this connection it is interesting to note that the usual procedure for introducing an zV-cyclopropylmethyl group5 (acylation by cyclopropanecarboxylic acid chloride followed by LAH reduction of the resulting amide) is inapplicable to 12 since the product, quite predictably, is 18.…”

mentioning

confidence: 99%

Analgesic 1-oxidized-2,6-methano-3-benzazocines

Michne¹,

Albertson²

1972

J. Med. Chem.

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mentioning

confidence: 99%

Analgesic 1-oxidized-2,6-methano-3-benzazocines

Michne¹,

Albertson²

1972

J. Med. Chem.

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“…Direct condensation of phenols with carbonyl compounds is one of the most general yet effective ways to prepare bis-phenols. The condensation of phenols with carbonyl compounds can be performed in mineral acids, − heteropolyacids as catalysts (e.g., phosphotungstic acid, H 3 PW 12 O 40 ·25H 2 O), cation exchange resin as catalyst (such as DOWEX 50WX4), with base, − or under photochemical conditions …”

Section: General Description Of Bis-phenolsmentioning

confidence: 99%

Supramolecular and Host−Guest Chemistry of Bis-phenol and Analogues

and

Baruah

2007

Crystal Growth & Design

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Recent developments on structural studies of bis-phenols and related compounds are systematically discussed. The effects of substituents on bis-phenols to control the size and shape of cavities in assemblies of bis-phenols and the weak interactions in anion-assisted assemblies of bis-phenols are narrated to illustrate pseudo-polymorphism. The possible impact of the occurrence of a high Z′ value in different polymorphs of bis-phenol and related compounds is presented.

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“…The residue was dissolved in benzene, the solution washed with water, and the solvent removed. The residue distilled a t 160-162" (0.5 mm) and the distillate (12 g or 77%) when crystallized from methanol melted a t 42-43" alone or in admixture with bis(p-chlorophenylmercapto)methane (8).…”

Section: Experiyiientalmentioning

confidence: 99%

Ω-Haloalkyl AND Ω -AMINOALKYL SULPHIDES CLEAVAGE OF THE ALKYL–SULPHUR BOND

Kulka¹

1959

Can. J. Chem.

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In the homologous series of p-chlorophenyl w-chloroalkyl sulphides (I), the first and second members reacted abnormally with amines to yield 1,w-bis(p-chlorophenylmercapto)allcanes (11). The fourth member of the series reacted 11ormally to produce 4-aminobutyl p-chlorophenyl sulphidc (111). The formation of I1 is explained on the basis of an alkyl-sulphur bond cleavage. The members of the p-chlorobenzyl series (VI) in general reacted with a~nines to form the cspected aminoalkyl sulphides (VII). However, the p-chlorobenzpl chloroalkpl sulphides (VI) were thermally labile and decomposed to p-chlorobenzpl chloride and a sulphur component. A cyclic sulphur component originated from VI whose chloroalkpl carbon chain was 4, 5, or 6. The thermal degradation of VI is explained t h r o~~g h a s~~lphonium salt cleavage. INTRODUCTIONI t has been recently shown that p-chlorophenyl chloro~nethyl sulphide (I, n = 1) can undergo an unusual bin~olecular reaction to form 2,8-dichloro-GH,12H-dibenzo(b,f)-1,sdithiocil~ (1). Now another anomalous reaction of I has been discovered and is the subject ~il.ianuscript receioed Septcnzber 18, 1058.

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Aldehyde—Phenol Reaction Products and Derivatives

Cited by 25 publications

References 0 publications

Analgesic 1-oxidized-2,6-methano-3-benzazocines

Analgesic 1-oxidized-2,6-methano-3-benzazocines

Supramolecular and Host−Guest Chemistry of Bis-phenol and Analogues

Ω-Haloalkyl AND Ω -AMINOALKYL SULPHIDES CLEAVAGE OF THE ALKYL–SULPHUR BOND

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