Metamaterials have gained much attention due to their exciting characteristics and potential uses in constructing valuable technologies. This paper presents a double negative square resonator shape metamaterial sensor to detect the material and its thickness. An innovative double-negative metamaterial sensor for microwave sensing applications is described in this paper. It has a highly sensitive Q-factor and has good absorption characteristics approximately equal to one. For the metamaterial sensor, the recommended measurement is 20 by 20 mm. Computer simulation technology (C.S.T.) microwave studios are used to design the metamaterial structure and figure out its reflection coefficient. Various parametric analyses have been performed to optimize the design and size of the structure. The experimental and theoretical results are shown for a metamaterial sensor that is attached to five different materials such as, Polyimide, Rogers RO3010, Rogers RO4350, Rogers RT5880, and FR-4. A sensor’s performance is evaluated using three different thicknesses of FR-4. There is a remarkable similarity between the measured and simulated outcomes. The sensitivity values for 2.88 GHz and 3.5 GHz are 0.66% and 0.19%, respectively, the absorption values for both frequencies are 99.9% and 98.9%, respectively, and the q-factor values are 1413.29 and 1140.16, respectively. In addition, the figure of merit (FOM) is analyzed, and its value is 934.18. Furthermore, the proposed structure has been tested against absorption sensor applications for the purpose of verifying the sensor's performance. With a high sense of sensitivity, absorption, and Q-factor, the recommended sensor can distinguish between thicknesses and materials in various applications.