A solvent-free synthesis of 4-aryl-
            <i>NH</i>
            -1,2,3-triazoles from ketones utilizing diphenyl phosphorazidate

Ishihara, Kotaro; Ishihara, Kazuki; Kato, Yamato; Shibuya, Shota; Shioiri, Takayuki; Matsugi, Masato

doi:10.1080/00397911.2022.2086466

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2022

2023

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“…The last topic utilizing DPPA we achieved very recently is the synthesis of 4-aryl- NH -1,2,3-triazoles 301 from benzyl-type ketones 300 in the presence of DBU, as shown in Scheme 53. 110 The work-up procedure of this synthesis is quite simple and the reaction efficiently proceeds in a short time. One of the characteristic nature of the reaction is that no solvent is required.…”

Section: Discussionmentioning

confidence: 99%