The development of light-weight and high-strength materials have gained attention to meet the evergrowing demands for safer and fuel-efficient automobiles. Thus, the importance and applications of composite materials are gradually increasing [1]. In the field of metal-matrix composite manufacturing, reinforcing agents are added to the metal matrix in the form of powders, whiskers, and fibers to improve the mechanical properties of metals [2]. Fibers have been used since the 1950s as structural reinforcements to develop metal-matrix composites. However, the improvements in physical properties in terms of high strength under extreme conditions have not yet been achieved. Thus, research into versatile reinforcements such as carbon fibers (CFs) has been conducted. Choi et al. [3] developed and processed CFs from polyacrylonitrile precursor materials. The resulting polyacrylonitrile-based CFs are still used in a wide-variety of applications since they exhibit excellent elasticity with strength 10 times higher and density 1/5 less than those of steel. Aluminum (Al), on the other hand, is commonly used as an engineering material since it is abundant on the earth's crust and is lightweight (2.7 g/cm 3 ). Additionally, it can easily form an alloy with other metals at low or high temperatures with high ductility and corrosion resistance [4].In practical applications, metal-matrix composites have failed to demonstrate promising results in terms of high strength and tribological properties. Such challenges arise from issues with uniform distribution of reinforcing agents throughout the metal-matrix during processing. Thus, most of the research and studies have focused on the homogenous features of metal-matrix composite processing to improve the tribological behavior. For instance, it has been confirmed that dispersing CFs throughout the polymer [5,6], ceramic [7][8][9], and metal [10-13] matrices reduce the overall friction coefficients and wear rates. While most research has emphasized the importance of processing parameters (such as wt% of CF in the matrix) in achieving low friction traits, it is also crucial to study the influence of structural modifications on the mechanical properties of composites. This is because one could easily assume that low-fiction materials exhibit a low shear strength (e.g., graphite). However, that is not the case for CF-reinforced Al composites. Godet [14] have suggested an alternate scenario of friction characteristics being involved in the formation of third bodies (phases) by using two parent materials [15]. The third bodies are usually shown as a thin film produced by the friction between the two parent materials; they accommodate the relative motion between the two bodies by transmitting stress. Thus, the formation of third bodies (transfer films) is a key to improving the overall tribological properties of CF-Al composites.In this study, CF-Al composites were produced through spark plasma sintering (SPS). The SPS method has the advantage of preventing grain growth during the high tem...