A new purge-and-membrane mass spectrometric (PAM-MS) instrument for analysis of volatile organic compounds in soil samples

Ojala, Marja; Mattila, Ismo; Särme, Timo; Ketola, Raimo A.; Kotiaho, Tapio

doi:10.1039/a905106f

Cited by 21 publications

(30 citation statements)

References 10 publications

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“…Sheet silicone membranes are often coupled with soil sampling devices that can be heated or purged. Purge-and-membrane mass spectrometry (PAM-MS) 49,169,170 and headspace MIMS (HS-MIMS) 171 are two ex situ techniques that combine the major advantages of headspace methods and membrane pervaporation for the direct determination of VOCs in soil samples.…”

Section: Soil Analysismentioning

confidence: 99%

Environmental applications of membrane introduction mass spectrometry

Ketola¹,

Kotiaho²,

Cisper³

et al. 2002

J. Mass Spectrom.

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154

121

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The purpose of this review is to highlight the versatility of membrane introduction mass spectrometry (MIMS) in environmental applications, summarize the measurements of environmental volatile organic compounds (VOCs) accomplished using MIMS, present developments in the detection of semi-volatile organic compounds (SVOCs) and forecast possible future directions of MIMS in environmental applications.

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Section: Soil Analysismentioning

confidence: 99%

Environmental applications of membrane introduction mass spectrometry

Ketola¹,

Kotiaho²,

Cisper³

et al. 2002

J. Mass Spectrom.

Self Cite

154

121

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“…(147). An analytical method has been developed by Meesters and Schröder (148) for simultaneous extraction and determination of two estrogenic active agents, 4-nonylphenol and bisphenol A, in residual activated mud and stabilized residual anaerobic mud.…”

Section: Soils Monitoringmentioning

confidence: 99%

Process Analytical Chemistry—Application of Mass Spectrometry in Environmental Analysis: An Overview

Llamas

Ojeda

Rojas

2007

Applied Spectroscopy Reviews

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“…However, MIMS is not suitable for solid samples. Purge-and-membrane mass spectrometry (PAM-MS), which combines dynamic headspace sampling and membrane inlet mass spectrometry (141)(142)(143)(144) has proved to be very promising for the analysis of VOCs in soil samples. Ojala et al (145) described a detailed evaluation of the suitability of the PAM-MS method for analysis of VOCs from soil samples and compares the method with HS-GC.…”

Section: Determination Of Mtbe In Soilsmentioning

confidence: 99%

State of the Art in the Determination of MTBE in Natural Waters and Soils

Atienza

Aragón

Herrero

et al. 2005

Critical Reviews in Analytical Chemistry

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Methyl tert-buthyl ether (MTBE) is used as an oxygenate additive in gasoline, and in the last years contamination of natural water, soils or air has taken place as result of MTBE use. Furthermore, MTBE is the second most common volatile compound (VOC) detected in a survey of shallow urban aquifers. This review focuses on the most critical steps, for sample preparation methodologies from an analytical point of view. Several enrichment and injection techniques are discussed, including direct injection, headspace analysis, purge and trap and solid-phase microextraction. The methods for the determination of methyl tert-butyl ether (MTBE) in environmental samples have been rapidly developed during last decade. Also, the current status of the analytical methods used in the determination of MTBE in water and soil is reviewed including the compound-specific stable isotope analysis (CSIA), which is an important tool in environmental sciences and allows the allocation of contaminant sources.

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A new purge-and-membrane mass spectrometric (PAM-MS) instrument for analysis of volatile organic compounds in soil samples

Cited by 21 publications

References 10 publications

Environmental applications of membrane introduction mass spectrometry

Environmental applications of membrane introduction mass spectrometry

Process Analytical Chemistry—Application of Mass Spectrometry in Environmental Analysis: An Overview

State of the Art in the Determination of MTBE in Natural Waters and Soils

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