A multinuclear double-tuned probe for applications with solids or liquids utilizing lumped tuning elements

Doty, F. David; Inners, Ruth R.; Ellis, Paul D.

doi:10.1016/0022-2364(81)90051-2

Cited by 54 publications

(42 citation statements)

References 2 publications

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“…The scroll coil is incorporated into the circuit diagrammed in Figure 2, which is an updated version of the original Cross et al (15) circuit and is similar to those used in other applications (16)(17)(18)(19)(20)(21) The circuit is double-tuned to 500 MHz ( 1 H) and 202 MHz ( 31 P). Two variable capacitors (Polyflon NRP/VC10-12-06A, www.polyflon.com) are used in both the 1 H and 31 P tuning networks, indicated as C2 and C3 for the 1 H channel and C6 and C7 for the 31 P channel.…”

Section: Resultsmentioning

confidence: 99%

An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil

Grant¹,

Sit²,

Angelis³

et al. 2007

Journal of Magnetic Resonance

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The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of 1 H and 31 P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.

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Section: Resultsmentioning

confidence: 99%

An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil

Grant¹,

Sit²,

Angelis³

et al. 2007

Journal of Magnetic Resonance

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“…The L B , L C , C B , and C C were calculated in accordance with Eqs. [6], [7], [8], and [9]. As a result, the L B was 67 nH, and the L C was 83 nH.…”

Section: Methodsmentioning

confidence: 99%

Double-tuned Radiofrequency Coil for 19F and 1H Imaging

et al. 2014

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“…19 F NMR experiments can possibly identify fluorine-containing compounds that are discriminable from the PVDF binder signal. [8][9][10] Correlations between the quantity of LiF on the cathode with respect to the number of cycles and the percentage of lithium loss from the cathode can be obtained.…”

mentioning

confidence: 99%

“…11 We designed, constructed, and tested an 7 Li and 19 F doubleresonance 600-MHz solid-state NMR probe with a solenoidal coil using a Cross-Waugh circuit. [12][13][14] Experimental Methods Probe Design and Probe Construction. The previously reported model for the design of a simple and effective probe was adapted, because the probe, which is the important interface between all NMR samples and the magnet fields resulting from RF pulses, has the strongest effects on the entire performance of the experiments.…”

mentioning

confidence: 99%

“…The probe utilized a solenoid coil, as in most solid-state NMR probes, and the two channels ( 7 Li and 19 F) used a CrossWaugh circuit for the double-tuned configuration. [18][19][20] The lithium ion battery for in-situ analysis had dimensions of 1.2 mm × 4 mm × 1 mm. A 7-turn round solenoidal coil with an ID of 5 mm and length of 15 mm was made from antique copper (Parawire, USA).…”

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Development of 600-MHz¹⁹F-⁷Li Solid-State NMR Probe for In-Situ Analysis of Lithium Ion Batteries

Jeong¹,

Park

Choi³

et al. 2013

Bulletin of the Korean Chemical Society

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Lithium is a highly attractive material for high-energy-concentration batteries, since it has low weight and high potential. Rechargeable lithium-ion batteries (LIBs), which have the extremely high gravimetric and volumetric energy densities, are currently the most preferable power sources for future electric vehicles and various portable electronic devices. In order to improve the efficiency and lifetime, new electrode compounds for lithium intercalation or insertion have been investigated for rechargeable batteries. Solid-state nuclear magnetic resonance (NMR) is a very useful tool to investigate the structural changes in electrode materials in actual working lithium-ion batteries. To detect the in-situ microstructural changes of electrode and electrolyte materials, 7 Li-19 F double-resonance solid-state NMR probe with a static solenoidal coil for a 600-MHz narrowbore magnet was designed, constructed, and tested successfully.

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A multinuclear double-tuned probe for applications with solids or liquids utilizing lumped tuning elements

Cited by 54 publications

References 2 publications

An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil

An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil

Double-tuned Radiofrequency Coil for 19F and 1H Imaging

Development of 600-MHz¹⁹F-⁷Li Solid-State NMR Probe for In-Situ Analysis of Lithium Ion Batteries

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A multinuclear double-tuned probe for applications with solids or liquids utilizing lumped tuning elements

Cited by 54 publications

References 2 publications

An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil

An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil

Double-tuned Radiofrequency Coil for 19F and 1H Imaging

Development of 600-MHz19F-7Li Solid-State NMR Probe for In-Situ Analysis of Lithium Ion Batteries

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Development of 600-MHz¹⁹F-⁷Li Solid-State NMR Probe for In-Situ Analysis of Lithium Ion Batteries