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Шемарова, И. В.; Maizel, E. B.; Voznyi, I. V.; Stepanova, N. P.; Khovanskikh, A. E.

doi:10.1023/a:1010355129735

Cited by 10 publications

(3 citation statements)

References 5 publications

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“…Calcd. for C 24 H 21 N 5 O 2 : C,70.06;H,5.14;N,17.02%;Found: C,70.42;H,5.43;N,16 ,5.17;N,14.36%;Found: C,73.59;H,5.48;N,14.59%.…”

Section: Preparation Of Ligandsmentioning

confidence: 98%

“…Preparation of PPeAP-INH [16] PPeAP (2.923 g, 10 mmol) was solved in ethanol (20 mL) at 80°C, to this solution was added INH (1.372 g, 10 mmol) and the mixture was refluxed for 3 h. Upon cooling to room temperature, the red solid was obtained from the mixture. The precipitated product was filtered, dried in air, and purified by recrystallization from ethanol.…”

Section: Preparation Of Ligandsmentioning

confidence: 99%

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Syntheses, crystal structures and thermal behavior of three Mn(II) complexes with 4-acyl pyrazolone derivatives

et al. 2007

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Three new manganese complexes, [Mn(PPeAP-INH)(CH 3 OH) 2 ] n (CHCl 3 ) (1) [PPeAP-INH=N-(1-phenyl-have been prepared, aiming at the formation of extended coordination polymer with Mn(II) ions. Formation of the corresponding manganese-ligand complexes has been monitored and characterized by chemical and spectroscopic techniques. X-ray diffraction analyses of available single crystals revealed 1D polymeric patterns of supramolecular system. Among them, the dimers of 2 and 3, bridged by two methanol molecules, are extended by hydrogen bond of O-HÁÁÁN to form the 1D chain. In these three new complexes which are all octahedral coordination environments, the N(5) atom of the pyridine heterocycles plays a very important role in building the bridged polymeric chain.

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“…Calcd. for C 24 H 21 N 5 O 2 : C,70.06;H,5.14;N,17.02%;Found: C,70.42;H,5.43;N,16 ,5.17;N,14.36%;Found: C,73.59;H,5.48;N,14.59%.…”

Section: Preparation Of Ligandsmentioning

confidence: 98%

Section: Preparation Of Ligandsmentioning

confidence: 99%

Syntheses, crystal structures and thermal behavior of three Mn(II) complexes with 4-acyl pyrazolone derivatives

et al. 2007

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“…New types of chemotherapeutic agents containing Schiff bases have generated tremendous interest among biochemists and some aminopyridines are commonly administered intravenously for the diagnosis of liver diseases in clinical practice [19][20][21][22]. To probe their chemotherapeutic functions, applications and properties, several 4-aminoantipyrine based agents are routinely administered intravenously for the diagnosis of liver diseases at diagnostic centers [23]. Chromosensors are widely used for environmental monitoring and in industrial and biological processes; consequently, research efforts are now being directed toward designing and developing sensitive yet simple 4-aminoantipyrine based chromosensors.…”

Section: Introductionmentioning

confidence: 99%

Synthesis, Spectral Characterization, Docking Analysis, DNA Binding/Cleavage, Antimicrobial and Cytotoxic Activity of New Dimeric Antipyrine-Schiff Base Metal Complexes

Alaghaz¹,

Alturiqi²,

Ammar³

et al. 2018

Asian J. Chem.

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In the present study, a new series of novel Schiff base ligand derived from (furan-2-carbaldehyde and 4-aminoantipyrine) and dimeric metal(II) complexes with the composition of [MLCl2]2, where M=Cu(II), Co(II), Ni(II) and Zn(II) have been synthesized and characterized by elemental analysis, magnetic susceptibility, molar conductivity measurements, FT-IR, UV-visible, 1 H NMR, 13 C NMR, EPR, MS (ESI), XRD, SEM and EDX studies. The spectral data recommend that the dimeric metal complexes embrace octahedral geometry around the central metal ions. The DMF solutions of the dimeric metal complexes demonstrate the lower molar conductance values which might be due to the non-electrolytic nature of the complexes (5.67-13.24 Ω -1 mol -1 cm -2 ). The biological studies involved are DNA interaction (binding and damage) antimicrobial, anti-proliferative and molecular docking. DNA interaction of these complexes carried out with using calf thymus DNA (CT-DNA) by electronic absorption titration, viscometric measurement which revealed that the synthesized dimeric complexes interact with DNA through intercalative binding mode. A gel electro-phoresis assay testifies the ability of complexes to cleave supercoiled pUC19 DNA in the presence of hydrogen peroxide as an activator. The synthesized compounds were initiated from their biological perspective. The antimicrobial assay indicates that dimeric complexes are good antimicrobial agents. Besides, in vitro antiproliferative activity of dimeric complexes were investigated on MCF-7, Hep G2, HBL-100 cell lines using an MTT assay. In addition, the molecular docking study was accomplished to considerate the nature of binding of the synthesized compounds with protein and DNA.

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Syntheses, crystal structures and thermal behaviors of three complexes with 4-acyl pyrazolone derivatives

Yang

Zhang

Liu

et al. 2007

Inorganica Chimica Acta

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Cited by 10 publications

References 5 publications

Syntheses, crystal structures and thermal behavior of three Mn(II) complexes with 4-acyl pyrazolone derivatives

Syntheses, crystal structures and thermal behavior of three Mn(II) complexes with 4-acyl pyrazolone derivatives

Synthesis, Spectral Characterization, Docking Analysis, DNA Binding/Cleavage, Antimicrobial and Cytotoxic Activity of New Dimeric Antipyrine-Schiff Base Metal Complexes

Syntheses, crystal structures and thermal behaviors of three complexes with 4-acyl pyrazolone derivatives

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