“…Each of the 18 bags was carefully labelled, so that the reaction histories could be easily identified, then three reaction flasks were set up: * Flask 1: Building block 29 a was added to bags 1, 2 and 3. * Flask 2: Building block 29 b was added to bags 4,5,6,7,8 and 9. * Flask 3: Building block 29 c was added to bags 10, 11, 12, 13, 14, 15, 16, 17 and 18. After 12 hours at 65 8C a sample of the polymer support was tested for free alkyne groups by placing a small amount of the polymer support (swollen with carbon tetrachloride) between two NaCl plates and recording the IR spectrum.…”