Greener, Efficient and Catalyst-Free Ultrasonic-Assisted Protocol for the<i>N</i>-Fmoc Protection of Amines

Mansouri, Rachida; Aouf, Zineb; Lakrout, Salah; Berredjem, Malika; Aouf, Nour-Eddine

doi:10.5935/0103-5053.20150286

Search citation statements

Order By: Relevance

Paper Sections

Select...

Results1

Citation Types

Supporting

Mentioning

Contrasting

Year Published

2016

2020

Publication Types

Select...

Article3

Relationship

Self Cite1

Independent2

Authors

Journals

Cited by 3 publications

(1 citation statement)

References 1 publication

Supporting

Mentioning

Contrasting

Order By: Relevance

“…Following our efforts to develop novel methods for acylation [24][25][26][27]12 and in continuation of our investigation on the use of ultrasound irradiation to accelerate reactions [28][29][30] , we describe a novel method for acylation the different amines and sulfonamides with acetic anhydride under ultrasonic irradiation, in absence of solvent and catalyst.…”

Section: Resultsmentioning

confidence: 99%

A Novel and Green Method for N-acylation of Amines and Sulfonamides under Ultrasound Irradiation

Bouasla¹,

Bechlem²,

Belhani³

et al. 2017

Orient. J. Chem

Self Cite

View full text Add to dashboard Cite

A facile and versatile method for acylation of structurally diverse amines and sulfonamides under focused ultrasonic irradiation in catalyst-free and solvent-free conditions is reported. There are several advantages to this approach such as simple and easier workup conditions, small amount of time and high yielding. The acylation reaction was carried out with acetic anhydride. All structures of synthesized products have been identified by NMR and mass spectroscopy.

show abstract