2018
DOI: 10.1590/s1517-707620180003.0506
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Comparativo entre o teste de Vicat e a calorimetria semi-adiabática para determinação do tempo de início e fim de pega em cimentos Portland

Abstract: RESUMO O objetivo deste trabalho foi de comparar dois métodos (Agulha de Vicat e Calorimetria Semi-Adiabática) para determinar o tempo de início e fim de pega do cimento Portland. Foram coletadas 10 amostras de 2 tipos de cimento com maior emprego na região sul do país de uma mesma unidade de fabricação, durante o mesmo mês. Verificou-se que o método de calorimetria semi-adiabática é uma técnica eficaz, prática e simples para monitorar o comportamento do processo de hidratação do cimento e fornecer resultados … Show more

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Cited by 4 publications
(5 citation statements)
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“…The greatest differences between the three methods evaluated were obtained for the final setting times, as shown in Figure 11. These differences are due to the fact that the tangent method consider the end of the setting process only when the temperature reaches the maximum peak after the period of induction [27], [29], [49], while in the other methods the end is considered before, being located close to the half of the period of acceleration [26], [50], [51]. In all of the correlations for final setting times, coefficients (r) very close to 1.0 were obtained, demonstrating and excellent correlation between the different methods.…”
Section: Comparison Between the Methods Of Determination Of The Settimentioning
confidence: 99%
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“…The greatest differences between the three methods evaluated were obtained for the final setting times, as shown in Figure 11. These differences are due to the fact that the tangent method consider the end of the setting process only when the temperature reaches the maximum peak after the period of induction [27], [29], [49], while in the other methods the end is considered before, being located close to the half of the period of acceleration [26], [50], [51]. In all of the correlations for final setting times, coefficients (r) very close to 1.0 were obtained, demonstrating and excellent correlation between the different methods.…”
Section: Comparison Between the Methods Of Determination Of The Settimentioning
confidence: 99%
“…The thermocouple wire was connected to the data collector ( Figure 3f). Based on the data obtained, three distinct methods were used for the analysis and determination of the initial and final setting times: the tangent method [46], direct fraction method [26], [47] and the derivatives method [48]. In each of the methods the times considered for each mixture was the arithmetic mean between the three samples tested.…”
Section: Mortarmentioning
confidence: 99%
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“…O calor de hidratação é uma propriedade importante de ser avaliada, pois influencia diretamente nos aspectos de trabalhabilidade e fluidez das pastas de cimento. É possível avaliar a reatividade dos cimentos Portland a partir das informações da taxa de calor [16]. A taxa de liberação de calor de hidratação, que ocorre após a mistura de uma pasta cimentícia, caracteriza-se por fases distintas.…”
Section: Introductionunclassified
“…Schematic illustration of length change and heat flow as a function of setting time of a cementitious material having shrinkage compensation by ettringite formation (adapted from[24,86]). …”
mentioning
confidence: 99%